反应条件
1: acetoacetic acid methyl ester With sodium hydride in tetrahydrofuran; mineral oil
T=0°C; 0.5 h; Inert atmosphere;
2: With N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran; hexane; mineral oil
T=-78 - -65°C; 1 h;
3: trans,trans-2,4-decadienal in tetrahydrofuran; hexane; mineral oil
T=-78 - -45°C;
参考文献
Jahn, Ullrich; Dinca, Emanuela
Chemistry - A European Journal, 2009 , vol. 15, # 1 p. 58 - 62
