5-己基呋喃-2(5H)-酮合成路线 (共 16 条)
反应条件
1: 80 percent / piperidine / acetonitrile / 3 h / Ambient temperature
2: 81 percent / piperidine / acetonitrile / 2 h / Heating
3: H2O2/acetic acid
4: 76 percent / triethylamine / CHCl3 / Ambient temperature
View Scheme
参考文献
Tanikaga, Rikuhei; Nozaki, Yoshihito; Tanaka, Kazuhiko; Kaji, Aritsune
Chemistry Letters, 1982 , p. 1703 - 1706
反应条件
1: aq. HCl / dioxane / Heating
2: triethylamine / CHCl3 / Ambient temperature
View Scheme
参考文献
Tanaka, Kazuhiko; Wakita, Hisanori; Yoda, Hidemi; Kaji, Aritsune
Chemistry Letters, 1984 , p. 1359 - 1362
反应条件
1: n-butyllithium / tetrahydrofuran
2: p-TsOH / benzene / Heating
3: triethylamine / benzene / Ambient temperature
View Scheme
参考文献
Tanaka, Kazuhiko; Ootake, Kazuhiko; Imai, Keisuke; Tanaka, Nobuo; Kaji, Aritsune
Chemistry Letters, 1983 , p. 633 - 636
反应条件
Amberlyst A-21 in ethyl acetate
24 h;
参考文献
Ma, Jie; Wang, Si Hong; Guan, Rong Tian
Synthetic Communications, 2006 , vol. 36, # 9 p. 1229 - 1233
参考文献
Canonne, P.; Akssira, M.
Tetrahedron Letters, 1984 , vol. 25, # 32 p. 3453 - 3456
反应条件
Yield given. Multistep reaction;
参考文献
Alexandre, Christian; Chlyeh, Mohamed Amal; Rouessac, Francis
Journal of Chemical Research, Miniprint, 1984 , # 8 p. 2327 - 2342