顺-1,4-二醋酸基-2-丁烯合成路线 (共 51 条)
反应条件
Hoveyda-Grubbs type catalyst immobilized on mesoporous molecular sieve SBA-15 in toluene T=70°C;
参考文献
Pastva, Jakub; Cejka, Jiri; Zilkova, Nadezda; Mestek, Oto; Rangus, Mojca; Balcar, Hynek
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 378, p. 184 - 192
反应条件
Grubb's 2nd generation catalyst T=40°C; 12 h;
参考文献
Organic Letters, , vol. 4, # 11 p. 1939 - 1942
反应条件
Grubb's 2nd generation catalyst in toluene T=80°C; 1.5 h; Inert atmosphere;
参考文献
Schmidt, Bernd; Krehl, Stefan; Hauke, Sylvia
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5427 - 5435
反应条件
C45H64Cl2N3PRu in dichloromethane-d2 T=20 - 45°C; Inert atmosphere;
参考文献
Storvick, Jennifer M.; Ankoudinova, Evgenia; King, Brianne R.; Van Epps, Heather; O'Neil, Gregory W.
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5858 - 5861
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene 5 h; Ambient temperature;
参考文献
Crilley, Martine M. L.; Golding, Bernard T.; Pierpoint, Colin
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2061 - 2068
反应条件
tetrakis(triphenylphosphine) palladium(0) in dichloromethane T=20°C; 48 h;
参考文献
Chavez, Cesar Sandoval; Rudler, Henri; Parlier, Andree; Herson, Patrick
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5843 - 5846
反应条件
C45H64Cl2N3PRu in dichloromethane-d2 T=20 - 45°C; Inert atmosphere;
参考文献
Storvick, Jennifer M.; Ankoudinova, Evgenia; King, Brianne R.; Van Epps, Heather; O'Neil, Gregory W.
Tetrahedron Letters, 2011 , vol. 52, # 44 p. 5858 - 5861
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=70°C; Product distribution; Further Variations:Solvents;
参考文献
Bouquillon, Sandrine; Muzart, Jacques
European Journal of Organic Chemistry, 2001 , # 17 p. 3301 - 3305
反应条件
RuCl2(9-isobutyl-9-phosphabicyclo-[3.3.1]-nonane)2(3-phenylindenylidene) in dichloromethane
T=25°C; Inert atmosphere;
参考文献
Sauvage, Xavier; Zaragoza, Guillermo; Demonceau, Albert; Delaude, Lionel
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1934 - 1948
反应条件
RuCl2(9-isobutyl-9-phosphabicyclo-[3.3.1]-nonane)2(3-phenylindenylidene) in dichloromethane
T=25°C; Inert atmosphere;
参考文献
Sauvage, Xavier; Zaragoza, Guillermo; Demonceau, Albert; Delaude, Lionel
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 11-12 p. 1934 - 1948