1-(1-羟基环己基)丙酮合成路线 (共 3 条)
反应条件
tert.-butylhydroperoxide; silver hexafluoroantimonate; Pd(quinox)Cl2; water in dichloromethane T=0 - 20°C; Wacker oxidation; 6.5 h;
参考文献
McCombs, Jessica R.; Michel, Brian W.; Sigman, Matthew S.
Journal of Organic Chemistry, 2011 , vol. 76, # 9 p. 3609 - 3613
反应条件
1: in diethyl ether T=5°C; 16 h; 2: With dihydrogen peroxide in methanol T=0 - 20°C; pH=7;
参考文献
Cergol, Katie M.; Turner, Peter; Coster, Mark J.
Tetrahedron Letters, 2005 , vol. 46, # 9 p. 1505 - 1509
参考文献
Yoshioka,T. et al.
Bulletin of the Chemical Society of Japan, 1972 , vol. 45, p. 636 - 638