253185-03-4合成路线 （共 388 条）
参考文献
Gronnier, Colombe; Kramer, Soren; Odabachian, Yann; Gagosz, Fabien
Journal of the American Chemical Society, 2012 , vol. 134, # 2 p. 828 - 831
反应条件
hydrogen; [Rh(μ-Cl)(2,5-norbornadiene)]2; phosphinated polydiacetylene in n-heptane T=30°C; P=60800 Torr; 8 h;
参考文献
Okano, Tamon; Tsukiyama, Katsunori; Konishi, Hisatoshi; Kiji, Jitsuo
Chemistry Letters, 1982 , p. 603 - 606
反应条件
6 Aequivalente Lithium;
参考文献
Benkeser et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 854
参考文献
Halse
Journal fuer Praktische Chemie (Leipzig), 1915 , vol. <2> 92, p. 41
反应条件
1: With AlCl3, aluminium chloride in anhydrous dichloroethane T=20°C; 1 h; Heating / reflux; 2: With hydrogenchloride in anhydrous dichloroethane; water T=20°C; 0.166667 h;
参考文献
LUPIN LIMITED
Patent: WO2004/26848 A1, 2004 ;
Location in patent: Page 34 ;
反应条件
1: With aluminium trichloride in 1,2-dichloro-benzene T=20°C; 5 h; 2: in 1,2-dichloro-benzene T=185°C; 0.333333 h; microwave irradiation;
参考文献
Yin, Wei; Ma, Yuan; Xu, Jiaxi; Zhao, Yufen
Journal of Organic Chemistry, 2006 , vol. 71, # 11 p. 4312 - 4315
反应条件
bromine; iodine T=0°C;
参考文献
Balaganesan, Banumathy; Shen, Wen-Jian; Chen, Chin H.
Tetrahedron Letters, 2003 , vol. 44, # 30 p. 5747 - 5750
反应条件
thallium(III) oxide; trifluoroacetic acid; potassium bromide T=20°C; 6 h;
参考文献
Kozak
Chem. Zentralbl., 1907 , vol. 78, # I p. 1787
反应条件
bromine T=25°C; 20 h; Irradiation; Yield given;
参考文献
Bolton, Roger; Bhangar, Muhammad Iqbal; Williams, Gareth H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 5 p. 893 - 896
参考文献
Stock; Brown
Journal of the American Chemical Society, 1959 , vol. 81, p. 5615,5617, 5620
