253185-03-4合成路线 (共 388 条)
参考文献
de la Mare; Harvey
Journal of the Chemical Society, 1957 , p. 131,134
反应条件
1: AlCl3 / 45 °C 2: glacial acetic acid; acetic acid anhydride; HNO3 / 30 - 40 °C View Scheme
参考文献
Legge
Journal of the American Chemical Society, 1947 , vol. 69, p. 2079,2083
反应条件
AlCl3 in dichloromethane; Petroleum ether
参考文献
Firmenich SA
Patent: US5552379 A1, 1996 ;
反应条件
1: 73 percent / AlCl3 / CH2Cl2 / 4 h / Ambient temperature 2: 64 percent / concd H2SO4 / 2 h / 95 °C View Scheme
参考文献
Nishida, Jun-Ichi; Deno, Hironori; Ichimura, Satoru; Nakagawa, Tomohiro; Yamashita, Yoshiro
Journal of Materials Chemistry, 2012 , vol. 22, # 10 p. 4483 - 4490
反应条件
1: 47 percent / FeCl3, I2, Br2 / 12 h / Ambient temperature 2: 19 percent / dimethylformamide / 5 h / Heating View Scheme
参考文献
Cook, Michael J.; Dunn, Adrian J.; Gold, Andrew A.; Thomson, Andrew J.; Daniel, Mervyn F.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 1583 - 1590
反应条件
1: 1.) AlCl3, 2.) AlCl3 / 1.) room temperature, 19 h 2: 67 percent / HNO3 / acetic anhydride; acetic acid / 50 h / Ambient temperature View Scheme
参考文献
Okada, Tadashi; Karaki, Ichiro; Mataga, Noboru
Journal of the American Chemical Society, 1982 , vol. 104, # 25 p. 7191 - 7195
反应条件
hydroxylamine-o-sulphonic acid; iron(II) sulfate in water; acetic acid T=40°C; 2 h; k(PhtBu)/k(C6H6); Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 49, # 23 p. 4479 - 4482
反应条件
1: ZnCl2 / 60 °C / Einleiten von HCl 2: ethanol 3: aqueous sulfuric acid; acetic acid View Scheme
参考文献
Guan, Yong; Ding, Zhensheng; Wulff, William D.
Chemistry - A European Journal, 2013 , vol. 19, # 46 p. 15565 - 15571
反应条件
1: ZnCl2 / 60 °C / Einleiten von HCl 2: ethanol View Scheme
参考文献
Berg
Roczniki Chemii, 1934 , vol. 14, p. 1249,1252
Chem. Zentralbl., 1935 , vol. 106, # I p. 2807
反应条件
sulfuryl dichloride; dibenzoyl peroxide
参考文献
Truce; Bee; Alfieri
Journal of the American Chemical Society, 1949 , vol. 71, p. 752