2,3-二苯基-1,3-丁二烯合成路线 （共 101 条）
反应条件
in diethyl ether
2 h; Ambient temperature; Further byproducts given;
参考文献
Skibbe, Volker; Erker, Gerhard
Journal of Organometallic Chemistry, 1983 , vol. 241, # 1 p. 15 - 26
反应条件
tetra-n-butylammonium tetrafluoroborate; Ni(2,2'-bipyridyl)(carbon monoxide)2 in various solvent(s)
Ambient temperatureelectrolysis, -1.6 V, further catalyst; Product distributionMechanism;
参考文献
Garnier, L.; Rollin, Y.; Perichon, J.
Journal of Organometallic Chemistry, 1989 , vol. 367, p. 347 - 358
反应条件
potassium peroxodisulfate; 3 A molecular sieve
T=120°C; 24 h; Product distribution; Further Variations:ReagentsTemperaturesTime;
参考文献
Wagner; Brinker
Synthesis, 2001 , # 3 p. 376 - 378
反应条件
1: n-BuLi / 1.) THF, hexane, -30 deg C, 30 min, 2.) THF, -30 deg C, then 25 deg C, 1 h
2: 1.) CuBr / 1.) THF, 30 min 0 deg C, 2.) THF, 30 min, 25 deg C
View Scheme
参考文献
Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1980 , vol. 99, # 11 p. 340 - 343
反应条件
copper(I) bromide
1.) THF, 30 min 0 deg C, 2.) THF, 30 min, 25 deg C; Yield given. Multistep reaction;
参考文献
Kleijn, H.; Westmijze, H.; Meijer, J.; Vermeer, P.
Recueil: Journal of the Royal Netherlands Chemical Society, 1980 , vol. 99, # 11 p. 340 - 343
反应条件
in diethyl ether
2 h; Ambient temperature; Further byproducts given;
参考文献
Skibbe, Volker; Erker, Gerhard
Journal of Organometallic Chemistry, 1983 , vol. 241, # 1 p. 15 - 26
反应条件
Grubb's 2nd generation catalyst
参考文献
Hilt, Gerhard; Roesner, Stefan
Synthesis, 2011 , # 4 art. no. Z29110SS, p. 662 - 668
反应条件
in 1,2,4-trichloro-benzene
6 h; Reflux;
参考文献
Rys, Andrzej Z.; Schultz, Erwin K. V.; Harpp, David N.
Journal of Sulfur Chemistry, 2010 , vol. 31, # 5 p. 351 - 371
反应条件
in toluene
2.25 h; Heatingother aldehydes or ketones; MechanismProduct distribution;
参考文献
Doxsee,K.M.; Mouser,J.K.
Tetrahedron Letters, 1991 , p. 1687
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
2 h; Heating; Mechanism;
参考文献
Nakayama, Juzo; Shibuya, Masahiro; Ikuina, Yoji; Murai, Fumito; Hoshino, Masamatsu
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 149 - 156
