in neat (no solvent) heating in cooled copper tube (water) to 650°C; description of apparatus given;; condensed (liquid O2); passed through flasks containing H2O and hot aq. KOH; dried over P2O5;;
参考文献
S: MVol.B3, 83, page 1712 - 1714
Brauer, G., Handbuch der praeparativen anorganischen Chemie, 2. Aufl., Bd. 1, Stuttgart 1960, S. 166
Brauer, G., Handbuch der praeparativen anorganischen Chemie, Stuttgart 1954, S. 140
in neat (no solvent) byproducts: OF2; introduction of F2 into steel chamber, sulfur in compartments; detailed description of apparatus and handling given;; first passing through Ni (or Monel) tube (400°C); second Cu column (H2O sprayed); passed into steel column (containing carbon/Fe shavings; aq. NaOH sprayed); dried in column (containing solid NaOH, BaO or P2O5);;
参考文献
Industrial and Engineering Chemistry, , vol. 39, p. 421 - 423
S: MVol.B3, 83, page 1712 - 1714
Inorganic syntheses, Bd. 3, New York 1950, S. 119/123
