反应条件
in tetrahydrofuran byproducts: NaCl; Addn. of Cl2C(CPhCPh) soln. to soln. of Mn-complex at -20°C under N2, color changes immediately to red.; Filtn., concg., addn. of pentane to the filtrate, stirring (5 min), sepg. of dark red ppt., recrystn. (toluene/pentane), washing (pentane), drying in vac., elem. anal.;
参考文献
Kirchgaessner, Uwe; Piana, Hermann; Schubert, Ulrich
Journal of the American Chemical Society, 1991 , vol. 113, # 6 p. 2228 - 2232
