1-甲基-4-苯基-1H-喹啉-2-酮合成路线 （共 30 条）
反应条件
tris(4-methylphenyl)-phosphine; silver carbonate; palladium (II) bromide in N,N-dimethyl acetamide; toluene
T=150°C; 1 h; Sealed tubeInert atmosphereMicrowave irradiationSchlenk technique;
参考文献
Carrer, Amandine; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2044 - 2054
反应条件
bismuth(III) chloride in chlorobenzene
T=90°C; 96 h;
参考文献
Elliott, Mark C.; Wordingham, Stuart V.
Synlett, 2004 , # 5 p. 898 - 900
反应条件
hydroquinone in benzene
T=190°C; 24 h;
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
反应条件
1: 48 percent / 2 h / 170 °C
2: 88 percent / NaH / dimethylsulfoxide / Ambient temperature
3: 55 percent / hydroquinone / benzene / 24 h / 220 °C
View Scheme
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
反应条件
1: 2) NaH / 1) 160 deg C, 1 h, 2) DMSO, r.t., overnight
2: 24 percent / hydroquinone / benzene / 24 h / 190 °C
View Scheme
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
反应条件
silver(I) acetate; triphenylphosphine; palladium (II) bromide in N,N-dimethyl acetamide; toluene
T=150°C; 1 h; Sealed tubeInert atmosphereMicrowave irradiationSchlenk technique;
参考文献
Carrer, Amandine; Brion, Jean-Daniel; Messaoudi, Samir; Alami, Mouad
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 10 p. 2044 - 2054
反应条件
oxygen in benzene
Oxidation; 2 h;
参考文献
Quast, Helmut; Ivanova, Svetlana; Peters, Eva-Maria; Peters, Karl
European Journal of Organic Chemistry, 2000 , # 3 p. 507 - 520
反应条件
1: pyridine / CH2Cl2 / 0.5 h / 20 °C
2: 83 percent / NaH / tetrahydrofuran / 2.5 h / Heating
3: 84 percent / K2CO3 / dimethylformamide / 0.5 h / 70 °C
View Scheme
参考文献
Park, Kwanghee Koh; Lee, Jin Joo
Tetrahedron, 2004 , vol. 60, # 13 p. 2993 - 2999
反应条件
1: 83 percent / NaH / tetrahydrofuran / 2.5 h / Heating
2: 84 percent / K2CO3 / dimethylformamide / 0.5 h / 70 °C
View Scheme
参考文献
Park, Kwanghee Koh; Lee, Jin Joo
Tetrahedron, 2004 , vol. 60, # 13 p. 2993 - 2999
反应条件
1: 88 percent / NaH / dimethylsulfoxide / Ambient temperature
2: 24 percent / hydroquinone / benzene / 24 h / 190 °C
View Scheme
参考文献
Kaupp, Gerd; Gruendken, Eleonore; Matthies, Doris
Chemische Berichte, 1986 , vol. 119, # 10 p. 3109 - 3120
