1: 93 percent / N-bromosuccinimide / dimethylformamide / 2.5 h
2: 1.) 1.4 M butyl-lithium; 2.) methyl iodide / 1.) dry ether, hexane, -10 deg C, 10 min; 2.) -10 deg C to R.T., 1 h
View Scheme
参考文献
Cracknell, Mark E.; Kabli, Reda A.; McOmie, John F. W.; Perry, David H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 115 - 120
Bausch, Joseph W.; Gregory. Peter S.; Olah, George A.; Prakash, G.K. Surya; Schleyer, Paul v.R.; Segal, Gerald A.
Journal of the American Chemical Society, 1989 , vol. 111, # 10 p. 3633 - 3640