3-(吡咯啉-1-基磺酰)砒啶合成路线 （共 4 条）
反应条件
in benzene T=0°C; 0.5 h; Yield given;
参考文献
Woolven, Holly; Gonzalez-Rodriguez, Carlos; Marco, Isabel; Thompson, Amber L.; Willis, Michael C.
Organic Letters, 2011 , vol. 13, # 18 p. 4876 - 4878
反应条件
1.1: isopropylmagnesium chloride / tetrahydrofuran / 0.5 h / 20 °C 1.2: SO2 / tetrahydrofuran / 0.5 h / -40 °C 1.3: SO2Cl2 / tetrahydrofuran / -40 - 20 °C 2.1: 342 mg / tetrahydrofuran / 3 h View Scheme
参考文献
Pandya, Rina; Murashima, Takashi; Tedeschi, Livio; Barrett, Anthony G. M.
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8274 - 8276
反应条件
1: PCl5 / 3 h / Heating 2: benzene / 0.5 h / 0 °C View Scheme
参考文献
Breant, P.; Marsais, F.; Queguiner, G.
Synthesis, 1983 , # 10 p. 822 - 824
反应条件
n-butyllithium; diisopropylamine
1.) Et2O, -70 deg C, 1 h; 2.) Et2O, -70 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Breant, P.; Marsais, F.; Queguiner, G.
Synthesis, 1983 , # 10 p. 822 - 824
