1-(3-苯基-2-丙烯酰)-1H-1,2,3-苯并三唑合成路线 (共 7 条)
反应条件
triethylamine in tetrahydrofuran 4.5 h; Reflux; regioselective reaction;
参考文献
Wang, Xiaoxia; Wang, Wencun; Wen, Yihang; He, Liang; Zhu, Xiangming
Synthesis, 2008 , # 20 p. 3223 - 3228
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Singh, Kamal Nain; Kaur, Amarjit
Synthetic Communications, 2005 , vol. 35, # 22 p. 2935 - 2937
反应条件
sodium azide; FeCl3·6H2O in water; acetone T=20°C; 0.416667 h;
参考文献
Zhong, Zhiyun; Hu, Jieling; Wang, Xiaoxia; Liu, Junhua; Zhang, Longfeng
Synthetic Communications, 2011 , vol. 41, # 16 p. 2461 - 2467
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.5 h; Title compound not separated from byproducts;
参考文献
Singh, Kamal Nain; Kaur, Amarjit
Synthetic Communications, 2005 , vol. 35, # 22 p. 2935 - 2937
反应条件
1: 1,2,3-Benzotriazole With thionyl chloride in dichloromethane
T=20°C; 0.5 h;
2: 3-phenyl-2-propenoic acid in dichloromethane
T=20°C; 3 h;
参考文献
Aitken, R. Alan; Murray, Lorna
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9781 - 9783
反应条件
samarium (III) iodide in dichloromethane
T=20°C; 20 h;
参考文献
Wang, Xiaoxia; He, Liang; Li, Zhifang; Wang, Wencun; Liu, Junhua
Synthetic Communications, 2009 , vol. 39, # 5 p. 819 - 829
反应条件
samarium (III) iodide in dichloromethane
T=20°C; 12 h;
参考文献
Wang, Xiaoxia; He, Liang; Li, Zhifang; Wang, Wencun; Liu, Junhua
Synthetic Communications, 2009 , vol. 39, # 5 p. 819 - 829