(4-氯苯基)(哌啶-1-基)甲酮合成路线 (共 26 条)
反应条件
tert.-butylhydroperoxide; FeCl3·6H2O in water; acetonitrile T=85°C; Inert atmosphere;
参考文献
Gaspa, Silvia; Porcheddu, Andrea; De Luca, Lidia
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 23 p. 3803 - 3807
反应条件
1: triethylamine / diethyl ether 2: water; acetonitrile / 25 °C View Scheme
参考文献
Lee, Jong Pal; Bae, Ae Ri; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 6 p. 1907 - 1911
反应条件
dihydrogen peroxide; iron(II) chloride in acetonitrile T=20°C; 0.0833333 h; Green chemistry;
参考文献
Xu, Daqian; Wang, Wenfang; Miao, Chengxia; Zhang, Qiaohong; Xia, Chungu; Sun, Wei
Green Chemistry, 2013 , vol. 15, # 10 p. 2975 - 2980
反应条件
potassium chloride in ethanol T=25°C; pH=10.52; Kinetics; Further Variations:pH-valuesconcentrations;
参考文献
Im, Li-Ra; Jeon, Sang-Eun; Um, Ik-Hwan
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 4 p. 1153 - 1157
反应条件
1: triethylamine / diethyl ether 2: acetonitrile / 25 °C View Scheme
参考文献
Um, Ik-Hwan; Bae, Ae Ri
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7510 - 7515
反应条件
hydrogenchloride in dimethyl sulfoxide; acetonitrile T=25°C; Substitution; Kinetics;
参考文献
Um, Ik-Hwan; Min, Ji-Sook; Ahn, Jung-Ae; Hahn, Hyun-Joo
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5659 - 5663
反应条件
phosphate buffer; potassium chloride in ethanol; water T=25°C; pH=7.25; Kinetics; Further Variations:pH-values;
参考文献
Castro, Enrique A.; Aguayo, Raul; Bessolo, Jorge; Santos, Jose G.
Journal of Organic Chemistry, 2005 , vol. 70, # 19 p. 7788 - 7791
反应条件
water in dimethyl sulfoxide T=25°C; aminolysis; Kinetics;
参考文献
Um, Ik-Hwan; Min, Ji-Sook; Lee, Hye-Won
Canadian Journal of Chemistry, 1999 , vol. 77, # 5-6 p. 659 - 666
反应条件
in water; dimethyl sulfoxide T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Lee, Ji-Youn; Ko, Seung-Hak; Bae, Sun-Kun
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5800 - 5803
反应条件
in water; dimethyl sulfoxide T=25°C; Kinetics;
参考文献
Um, Ik-Hwan; Lee, Ji-Youn; Ko, Seung-Hak; Bae, Sun-Kun
Journal of Organic Chemistry, 2006 , vol. 71, # 15 p. 5800 - 5803