(S)-(+)-2-戊醇合成路线 (共 77 条)
反应条件
hydrogen; palladium on activated carbon; N-butylamine in methanol; water T=30°C; 50 h;
参考文献
DAISO CO., LTD.
Patent: EP1582511 A2, 2005 ;
Location in patent: Page/Page column 5 ;
反应条件
dried cells of Geotrichum candidum; nicotinamide adenine dinucleotide; isopropyl alcohol in various solvent(s) T=30°C; pH=7.0; 9 h; Enzymatic reaction;
参考文献
Matsuda, Tomoko; Nakajima, Yuta; Harada, Tadao; Nakamura, Kaoru
Tetrahedron Asymmetry, 2002 , vol. 13, # 9 p. 971 - 974
反应条件
Novozyme 435 in neat (no solvent) T=45°C; P=760.051 Torr; 12 h; Molecular sieveGreen chemistryEnzymatic reaction; enantioselective reaction;
参考文献
Ren, Liwei; Xu, Tian; He, Ruoping; Jiang, Zhenhua; Zhou, Hua; Wei, Ping
Tetrahedron Asymmetry, 2013 , vol. 24, # 5-6 p. 249 - 253
反应条件
Novozyme 435 in neat (no solvent) T=45°C; P=760.051 Torr; 8 h; Molecular sieveGreen chemistryEnzymatic reaction; TemperatureConcentrationTime; enantioselective reaction;
参考文献
Ren, Liwei; Xu, Tian; He, Ruoping; Jiang, Zhenhua; Zhou, Hua; Wei, Ping
Tetrahedron Asymmetry, 2013 , vol. 24, # 5-6 p. 249 - 253
反应条件
Novozyme 435 in neat (no solvent) T=45°C; P=760.051 Torr; 8 h; Molecular sieveGreen chemistryEnzymatic reaction; enantioselective reaction;
参考文献
Ren, Liwei; Xu, Tian; He, Ruoping; Jiang, Zhenhua; Zhou, Hua; Wei, Ping
Tetrahedron Asymmetry, 2013 , vol. 24, # 5-6 p. 249 - 253
反应条件
Novozyme 435 in neat (no solvent) T=45°C; P=760.051 Torr; 8 h; Molecular sieveGreen chemistryEnzymatic reaction; enantioselective reaction;
参考文献
Ren, Liwei; Xu, Tian; He, Ruoping; Jiang, Zhenhua; Zhou, Hua; Wei, Ping
Tetrahedron Asymmetry, 2013 , vol. 24, # 5-6 p. 249 - 253
反应条件
zinc(II) chloride in diethyl ether T=25°C; 1 h;
参考文献
Cheskis, B. A.; Shpiro, N. A.; Moiseenkov, A. M.
Journal of Organic Chemistry USSR (English Translation), 1990 , vol. 26, # 9.1 p. 1613 - 1616
Zhurnal Organicheskoi Khimii, 1990 , vol. 26, # 9 p. 1864 - 1869
反应条件
[14C]-D-Lactic acid durch Verestern, Rektifizieren und Verseifen;
参考文献
Pickard; Kenyon
Journal of the Chemical Society, 1913 , vol. 103, p. 1940,1935
Journal of the Chemical Society, 1911 , vol. 99, p. 55,64
Full Text Show Details
Pickard; Kenyon
Journal of the Chemical Society, 1911 , vol. 99, p. 55,71
Journal of the Chemical Society, 1914 , vol. 105, p. 1121,1123, 1128
反应条件
SADH from Thermoanaerobacter ethanolicus T=37°C; enantiospecificity in enzymatic reaction; var. temp.; Product distribution;
参考文献
Keinan,E.; Hafeli,E.K.; Seth,K.K.
Journal of the American Chemical Society, 1986 , vol. 108, p. 162
反应条件
anatase TiO2 supported Ru(OH)x in toluene T=79.84°C; P=760.051 Torr; 8 h; Inert atmosphere;
参考文献
Yamaguchi, Kazuya; Koike, Takeshi; Kim, Jung Won; Ogasawara, Yoshiyuki; Mizuno, Noritaka
Chemistry - A European Journal, 2008 , vol. 14, # 36 p. 11480 - 11487