1-(4-羟基-2,5-二甲基苯基)-乙酮合成路线 (共 4 条)
反应条件
aluminium trichloride in nitromethane T=50°C; Fries rearrangement; 12 h;
参考文献
Bakke, Brian A.; McIntosh, Matthias C.; Turnbull, Kenneth D.
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4338 - 4345
反应条件
1: 98 percent / triethylamine / CH2Cl2 / 12 h / 20 °C 2: 75 percent / AlCl3 / nitromethane / 12 h / 50 °C View Scheme
参考文献
Bakke, Brian A.; McIntosh, Matthias C.; Turnbull, Kenneth D.
Journal of Organic Chemistry, 2005 , vol. 70, # 11 p. 4338 - 4345
参考文献
Kindler et al.
Archiv der Pharmazie (Weinheim, Germany), 1954 , vol. 287, p. 210,223
反应条件
in methanol Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Suau, Rafael; Torres, Gregorio; Valpuesta, Maria
Tetrahedron Letters, 1995 , vol. 36, # 8 p. 1311 - 1314