in tetrahydrofuran (argon); NMR tube: addn. of the ligand to the Pt complex in THF at -78°C, slight warming for dissoln., recooling to -80°C; NMR monitoring;
参考文献
Chaloner, Penny A.; Broadwood-Strong, Gillian T. L.
Journal of the Chemical Society - Dalton Transactions, 1996 , # 6 p. 1039 - 1043
Abdur-Rashid, Kamaluddin; Fong, Tina P.; Greaves, Bronwyn; Gusev, Dmitry G.; Hinman, Justin G.; Landau, Shaun E.; Lough, Alan J.; Morris, Robert H.
Journal of the American Chemical Society, 2000 , vol. 122, # 38 p. 9155 - 9171
in benzene-d6 (N2); using Schlenk techniques; charging of NMR tube with Ru(CHPh)Cl2(C3N2H4Mes2)2, PCy3 (excess) and C6D6; heating at 80°C for 36 h; monitoring by NMR;
参考文献
Rosen, Evelyn L.; Sung, Daphne H.; Chen, Zheng; Lynch, Vincent M.; Bielawski, Christopher W.
Organometallics, 2010 , vol. 29, # 1 p. 250 - 256
