(S)-(-)- α-甲基苄胺合成路线 （共 369 条）
反应条件
sulfuric acid in water 2 h; Ambient temperature; Yield given;
参考文献
Ikota; Achiwa; Yamada
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 3 p. 887 - 894
反应条件
hydroxylammonium acetate in ethanol 10 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuanwei, Chen; Aiqiao, Mi; Xun, Xiao; Yaozhong, Jiang
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1423 - 1430
反应条件
hydroxylammonium acetate in ethanol 10 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Yuanwei, Chen; Aiqiao, Mi; Xun, Xiao; Yaozhong, Jiang
Synthetic Communications, 1989 , vol. 19, # 7,8 p. 1423 - 1430
反应条件
2: 2) Pb(OAc)4 / 1) THF, reflux, 2) CH2Cl2, MeOH View Scheme
参考文献
Wu, Ming-Jung; Pridgen, Lendon N.
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1340 - 1344
反应条件
BM-ωTA; ωTA ATA-117 102907WW; pyridoxal 5'-phosphate; pentan-3-one T=30°C; pH=7; 24 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Koszelewski, Dominik; Grischek, Barbara; Glueck, Silvia M.; Kroutil, Wolfgang; Faber, Kurt
Chemistry - A European Journal, 2011 , vol. 17, # 1 p. 378 - 383
反应条件
tert-butyl methyl ether 24 h; crude Burkholderia plantarii lipase; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Balkenhohl, Friedhelm; Ditrich, Klaus; Hauer, Bernhard; Ladner, Wolfgang
Journal fur Praktische Chemie - Chemiker - Zeitung, 1997 , vol. 339, # 4 p. 381 - 384
反应条件
in toluene T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Arseniyadis, Stellios; Subhash, Pithani V.; Valleix, Alain; Wagner, Alain; Mioskowski, Charles
Chemical Communications, 2005 , # 26 p. 3310 - 3312
反应条件
sodium 2-oxopropanoate T=30°C; pH=7.5; 48 h; aq. phosphate bufferEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Clay, Dorina; Koszelewski, Dominik; Grischek, Barbara; Gross, Johannes; Lavandera, Ivan; Kroutil, Wolfgang
Tetrahedron Asymmetry, 2010 , vol. 21, # 16 p. 2005 - 2009
反应条件
Chromobacterium violaceum ω-transaminase variant W60C T=37°C; pH=7; 12 h; Reagent/catalystpH-value; enantioselective reaction;
参考文献
Wang, Bo; Land, Henrik; Berglund, Per
Chemical Communications, 2013 , vol. 49, # 2 p. 161 - 163
反应条件
lead(IV) acetate 1) THF, reflux, 2) CH2Cl2, MeOH; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wu, Ming-Jung; Pridgen, Lendon N.
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1340 - 1344
