alpha-溴-4-甲氧基苯乙酮合成路线 （共 261 条）
反应条件
1: [Ru(II)(2,2’-bipyridine)3]Cl2; DNP; ascorbic acid powder / methanol; water / 15 h / Inert atmosphere; Irradiation 2: bromine / chloroform / 0 - 65 °C View Scheme
参考文献
Maji, Tapan; Karmakar, Ananta; Reiser, Oliver
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 736 - 739
反应条件
n-butyllithium; lithium diisopropyl amide Yield given. Multistep reaction;
参考文献
Kowalski, Conrad J.; Haque, M. Serajul
Journal of Organic Chemistry, 1985 , vol. 50, # 25 p. 5140 - 5142
反应条件
oxygen T=10°C; 2 h; Irradiation;
参考文献
Izawa; Ishiguro; Tomioka
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 5 p. 1490 - 1496
反应条件
hydrogen cation in water T=25°C; Rate constant;
参考文献
Soerensen, Poul E.; Loegager, Tine; Kanagasabapathy, V. M.; McClelland, Robert, A.
Bulletin de la Societe Chimique de France, 1988 , # 2 p. 313 - 316
参考文献
Grignard; Perrichon
Annales de Chimie (Cachan, France), 1926 , vol. <10> 5, p. 20
反应条件
carbon disulfide; aluminium trichloride
参考文献
Kunckell; Scheven
Chemische Berichte, 1898 , vol. 31, p. 173
反应条件
in xylene T=60°C; Ea; other solvents and temp., var. 1,2-dioxetanes; Thermodynamic dataRate constant;
参考文献
Richardson, William H.; Stiggal-Estberg, Diana L.; Chen, Zhangping; Baker, John C.; Burns, David M.; Sherman, David G.
Journal of Organic Chemistry, 1987 , vol. 52, # 14 p. 3143 - 3150
反应条件
1: 6 g / NaH / tetrahydrofuran / 0.5 h / Ambient temperature 2: acetic anhydride / 0.25 h / 40 °C View Scheme
参考文献
Ogata, Masaru; Matsumoto, Hiroshi; Kida, Shiro; Shimizu, Sumio; Tawara, Katsuya; Kawamura, Yoshimi
Journal of Medicinal Chemistry, 1987 , vol. 30, # 8 p. 1497 - 1502
参考文献
Corrigan et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 6258
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Sawa
Shionogi Kenkyusho Nenpo, 1952 , # 2 p. 104
Chem.Abstr., 1957 , p. 10423
反应条件
dimethyl sulfoxide in water T=50°C; 2.5 h;
参考文献
MITSUBISHI PHARMA CORPORATION; SANOFI-SYNTHELABO
Patent: WO2004/85408 A1, 2004 ;
Location in patent: Page 262 ;
WO 2004/085408 A1
