2,4,6-三甲基苯溴化镁合成路线 （共 186 条）
参考文献
Arnold; Liggett; Searles
Journal of the American Chemical Society, 1948 , vol. 70, p. 3938
反应条件
1.1: tetrahydrofuran / 3 h / 0 °C / |Inert atmosphere
1.2: 15 h / 0 - 20 °C / |Inert atmosphere
2.1: samarium diiodide; tert-butyl alcohol / tetrahydrofuran / -78 - 20 °C / |Inert atmosphere
View Scheme
参考文献
Schaefer, Sara L.; Roberts, Connor L.; Volz, Erasmus O.; Grasso, Monika R.; O'Neil, Gregory W.
Tetrahedron Letters, 2013 , vol. 54, # 45 p. 6125 - 6128
参考文献
Sokolowa; Dolgaja
Zhurnal Obshchei Khimii, 1956 , vol. 26, p. 534,536; engl. Ausg. S. 569, 570
参考文献
Burton; Munday
Journal of the Chemical Society, 1954 , p. 1456,1459
参考文献
Liberman et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1956 , p. 1000,1001, 1004; engl. Ausg. S. 1021, 1022, 1025
参考文献
Arnold; Liggett; Searles
Journal of the American Chemical Society, 1948 , vol. 70, p. 3938
反应条件
trichlorosilane in tetrahydrofuran
T=0 - 20°C; 39.75 h;
参考文献
Braddock-Wilking, Janet; Schieser, Matt; Brammer, Lee; Huhmann, Jean; Shaltout, Raef
Journal of Organometallic Chemistry, 1995 , vol. 499, # 1.2 p. 89 - 98
参考文献
McElvain; Davie
Journal of the American Chemical Society, 1951 , vol. 73, p. 1400
参考文献
McElvain; Venerable
Journal of the American Chemical Society, 1950 , vol. 72, p. 1661,1667
反应条件
PEPPSI™-IPr catalyst in tetrahydrofuran
T=50°C; Kumada-Tamao-Corriu reaction; 24 h;
参考文献
Total Synthesis, Ltd.
Patent: US2007/73055 A1, 2007 ;
Location in patent: Page/Page column 13-14; 20 ;
