2,4,6-三甲基苯溴化镁合成路线 (共 186 条)
反应条件
[(THF)4Li4(CH3)8Ni2] in tetrahydrofuran T=0°C; Kumada cross-coupling reaction; 26.5 h;
参考文献
Lamm, Katja; Stollenz, Michael; Meier, Mirko; Goerls, Helmar; Walther, Dirk
Journal of Organometallic Chemistry, 2003 , vol. 681, # 1-2 p. 24 - 36
反应条件
[(THF)4Li4(CH3)8Ni2] in tetrahydrofuran T=20°C; Kumada cross-coupling reaction; 96 h;
参考文献
Lamm, Katja; Stollenz, Michael; Meier, Mirko; Goerls, Helmar; Walther, Dirk
Journal of Organometallic Chemistry, 2003 , vol. 681, # 1-2 p. 24 - 36
反应条件
[(THF)4Li4(CH3)8Ni2] in tetrahydrofuran T=20°C; Kumada cross-coupling reaction; 4 h;
参考文献
Lamm, Katja; Stollenz, Michael; Meier, Mirko; Goerls, Helmar; Walther, Dirk
Journal of Organometallic Chemistry, 2003 , vol. 681, # 1-2 p. 24 - 36
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran T=0°C; 1 h; Inert atmosphere;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 36 p. 6731 - 6734
参考文献
Spielman; Schmidt
Journal of the American Chemical Society, 1937 , vol. 59, p. 2010
反应条件
arsenic(III) chloride; ethylene dibromide
参考文献
Ludwig; Dolny; Goetze
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 1997 , vol. 53, # 13 p. 2363 - 2372
参考文献
Zeon Corporation
Patent: EP1405840 A1, 2004 ;
Location in patent: Page 19 ;
反应条件
oxygen; lithium chloride; manganese (II) chloride in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
参考文献
Cahiez, Gerard; Duplais, Christophe; Buendia, Julien
Angewandte Chemie, International Edition, 2009 , vol. 48, # 36 p. 6731 - 6734
反应条件
palladium diacetate in tetrahydrofuran
T=60°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Organic Letters, 2006 , vol. 8, # 22 p. 5057 - 5060
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in tetrahydrofuran
T=60°C; 20 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Angewandte Chemie - International Edition, 2006 , vol. 45, # 14 p. 2289 - 2292