1,3-二噻烷1,1,3,3-四氧化物合成路线 （共 4 条）
反应条件
dihydrogen peroxide in water T=75°C; 3 h;
参考文献
Jereb, Marjan
Green Chemistry, 2012 , vol. 14, # 11 p. 3047 - 3052,6
Title/Abstract Full Text Show Details
Jereb, Marjan
Green Chemistry, 2012 , vol. 14, # 11 p. 3047 - 3052
反应条件
hydrogenchloride Oxydieren des Reaktionsprodukts mit Kaliumpermanganat in verd. Schwefelsaeure;
参考文献
Autenrieth; Wolff
Chemische Berichte, 1899 , vol. 32, p. 1373
反应条件
methanol; sodium methylate
1.) DMF, MeOH, 10 min, 2.) 70-80 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Li, Chuen; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1303 - 1310
反应条件
methanol; sodium methylate
1.) DMF, MeOH, 10 min, 2.) 70-80 deg C, 3 h; Yield given. Multistep reaction;
参考文献
Li, Chuen; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1303 - 1310
