1-氯-4-[1-(4-氯苯基)乙烯基]苯合成路线 (共 37 条)
反应条件
1: Behandeln des Reaktionsprodukts mit wss. Natriumcarbonat-Loesung
2: palladium-BaSO4; ethanol / Hydrogenation
View Scheme
参考文献
Bergmann et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 1612,1614
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in tetrahydrofuran
T=20°C;
参考文献
Lu, Bei-Li; Shi, Min
Chemistry - A European Journal, 2011 , vol. 17, # 33 p. 9070 - 9075
反应条件
tris(trifluoroacetoxy)-λ3-iodane in tetrachloromethane
T=23°C; 3 h;
参考文献
Futami; Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3182 - 3186
反应条件
1: 6 percent / Mn(OAc)2, O2 / acetic acid / 12 h / 23 °C
2: 68 percent / KOH / methanol / 12 h / Heating
3: 84 percent / 2 M aq. HCl / acetic acid / 0.33 h / 80 °C
View Scheme
参考文献
Qian, Chang-Yi; Yamada, Takashi; Nishino, Hiroshi; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1992 , vol. 65, # 5 p. 1371 - 1378
反应条件
air; acetic acid
T=23°C; 12 h; Further byproducts given;
参考文献
Nishino, Hiroshi; Tategami, Shin-ichi; Yamada, Takashi; Korp, James D.; Kurosawa, Kazu
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 6 p. 1800 - 1809
反应条件
1: acetic acid
2: Br2 / CHCl3
3: KOH / ethanol
View Scheme
参考文献
Sakla,A.B. et al.
Journal fuer Praktische Chemie (Leipzig), 1972 , vol. 314, p. 793 - 798
反应条件
tris(trifluoroacetoxy)-λ3-iodane in tetrachloromethane
T=23°C; 3 h;
参考文献
Futami; Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3182 - 3186