[1-(羟基甲基)环己基]甲醇合成路线 （共 27 条）
反应条件
lithium aluminium tetrahydride
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
反应条件
1: methyl cyclohexane-carboxylate With lithium diisopropyl amide in tetrahydrofuran T=-70°C; 4 h; Inert atmosphere; 2: methyl chloroformate in tetrahydrofuran T=-78 - 20°C; 3: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; Inert atmosphere;
参考文献
Nippon Carbide Industries Co., Inc.; Kakinuma, Shinichi; Murotani, Masahiro; Nakamori, Seijin
Patent: US2013/41184 A1, 2013 ;
Location in patent: Paragraph 0016; 0017 ;
反应条件
methanol; nickel T=45°C; P=51485.6 Torr; Hydrogenation;
参考文献
French; Gallagher
Journal of the American Chemical Society, 1942 , vol. 64, p. 1497
反应条件
1: 53 percent / NaOEt / ethanol 2: 89 percent / NaAlH2(OCH2OCH3)2 / tetrahydrofuran View Scheme
参考文献
Fajgar, Radek; Pola, Josef
Journal of Organic Chemistry, 1993 , vol. 58, # 27 p. 7709 - 7717
参考文献
Golding; Millar; Paul; Richards
Tetrahedron, 1993 , vol. 49, # 32 p. 7051 - 7062
参考文献
Backer; Winter
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 492,506
参考文献
Backer; Winter
Recueil des Travaux Chimiques des Pays-Bas, 1937 , vol. 56, p. 492,506
反应条件
sulfuric acid T=150 - 155°C; 12 h; Further byproducts given;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; Further byproducts given;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
反应条件
sulfuric acid T=150 - 155°C; 48 h; other substrates, other time, other concentration of H2SO4; MechanismProduct distribution;
参考文献
Molnar, Arpad; Bucsi, Imre; Bartok, Mihaly
Tetrahedron, 1992 , vol. 48, # 23 p. 4929 - 4936
