N,N-二乙基-2-丙烯酰胺合成路线 (共 23 条)
反应条件
nickel(II) cyanide; water; hydroquinone T=130°C;
参考文献
Reppe
Justus Liebigs Annalen der Chemie, 1953 , vol. 582, p. 1,13, 31
反应条件
diethyl ether unter vermindertem Druck;
参考文献
Goodrich Co.
Patent: GB648886 , 1947 ;
反应条件
T=506 - 520°C; Pyrolysis;
参考文献
Ratchford; Lengel; Fisher
Journal of the American Chemical Society, 1949 , vol. 71, p. 648,650
反应条件
(i) 4-dimethylamino-but-3-yn-2-one, THF, (ii) /BRN= 605268/; Multistep reaction;
参考文献
Neuenschwander,M. et al.
Helvetica Chimica Acta, 1978 , vol. 61, p. 2428 - 2436
反应条件
(i) POCl3, (ii) /BRN= 605268/; Multistep reaction;
参考文献
Bellasio,E. et al.
Gazzetta Chimica Italiana, 1968 , vol. 98, p. 1014 - 1030
参考文献
Abramov,V.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 2237 - 2240,2183 - 2185
反应条件
hydroquinone T=200°C; 8 h; other alkyl 3-(diethylamino)propionates, var. times; also in the presence of diethylamine or methyl acrylate; Product distributionMechanism;
参考文献
Kazantsev, O. A.; Zil'berman, E. N.; Shirshin, K. V.; Krasnov, V. L.; Salov, V. N.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 9.2 p. 1687 - 1691
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 9 p. 1914 - 1919
反应条件
T=200°C; with 1percent hydroquinone; other acrylate esters; diff. temp.; Product distributionMechanismKinetics;
参考文献
Kazantsev, O. A.; Zil'berman, E. N.; Salov, V. N.; Krasnov, V. L.; Shirshin, K. V.
J. Appl. Chem. USSR (Engl. Transl.), 1990 , vol. 63, # 8.1 p. 1756 - 1760,1621 - 1625
反应条件
in tetrahydrofuran T=-78°C;
参考文献
Knapp, Spencer; Calienni, John
Synthetic Communications, 1980 , vol. 10, # 11 p. 837 - 842
反应条件
[Pd2(dba)2]; oxygen in acetic acid
T=90°C; P=760.051 Torr; 16 h; chemoselective reaction;
参考文献
Harada, Seiichiro; Yano, Hiroki; Obora, Yasushi
ChemCatChem, 2013 , vol. 5, # 1 p. 121 - 125