3,5-二硝基苯甲酸甲酯合成路线 （共 42 条）
反应条件
1: 87 percent / PhP(O)Cl2; PCl5 / 15 h / Heating 2: 94 percent / NaOCH3 / 0 - 20 °C 3: 60 percent / HCl / acetone View Scheme
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 8 p. 684 - 686
反应条件
1: 3,5-dinitro benzoic acid With 2,4,6-trichloro-1,3,5-triazine; potassium carbonate in tetrahydrofuran; acetonitrile T=0°C; 2.75 h; 2: diazomethane in diethyl ether T=0 - 20°C; 12 h;
参考文献
Forbes; Barrett; Lewis; Smith
Tetrahedron Letters, 2000 , vol. 41, # 51 p. 9943 - 9947
反应条件
1: 94 percent / NaOCH3 / 0 - 20 °C 2: 60 percent / HCl / acetone View Scheme
参考文献
Monk, Keith A.; Siles, Rogelio; Pinney, Kevin G.; Garner, Charles M.
Tetrahedron Letters, 2003 , vol. 44, # 19 p. 3759 - 3761
反应条件
in dichloromethane T=10°C; 10 h; Yield given;
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 8 p. 684 - 686
反应条件
in methanol 3 h; Heating;
参考文献
Gloede, J.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 4 p. 667 - 668
反应条件
3-trimethylsilyl-2-oxazolidinone 0.25 h; Ambient temperature; Yield given;
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 8 p. 684 - 686
参考文献
Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 4 p. 1206 - 1213
反应条件
1: nitric acid; sulfuric acid; water / 14.84 °C 2: nitric acid; sulfuric acid; water / 69.84 °C View Scheme
参考文献
Di Somma, Ilaria; Marotta, Raffaele; Andreozzi, Roberto; Caprio, Vincenzo
Organic Process Research and Development, 2012 , vol. 16, # 12 p. 2001 - 2007
反应条件
in acetonitrile T=30°C; Activation energyKineticsThermodynamic data;
参考文献
Kondo, Yasuhiko; Urade, Miyuki; Yamanishi, Yukari; Chen, Xinyu
Journal of the Chemical Society, Perkin Transactions 2, 2002 , # 8 p. 1449 - 1454
反应条件
sulfuric acid; water; nitric acid T=69.84°C; Kinetics; ConcentrationTemperature;
参考文献
Di Somma, Ilaria; Marotta, Raffaele; Andreozzi, Roberto; Caprio, Vincenzo
Organic Process Research and Development, 2012 , vol. 16, # 12 p. 2001 - 2007
