[双(三氟乙酰氧基)碘]苯合成路线 (共 95 条)
反应条件
Oxonereg; in chloroform T=20°C; 1.2 h;
参考文献
Zagulyaeva, Aleksandra A.; Yusubov, Mekhman S.; Zhdankin, Viktor V.
Journal of Organic Chemistry, 2010 , vol. 75, # 6 p. 2119 - 2122
反应条件
sodium percarbonate in dichloromethane T=0 - 25°C; 20 h;
参考文献
Kazmierczak, Pawel; Skulski, Lech
Molecules, 2002 , vol. 7, # 11 p. 810 - 812
参考文献
Shabarov, Yu. S.; Pisanova, E. V.; Saginova, L. G.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1685 - 1689
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 9 p. 1886 - 1892
反应条件
mercury(II) oxide in chloroform 0.25 h; Ambient temperature;
参考文献
Taylor, Richard T.; Stevenson, Thomas A.
Tetrahedron Letters, 1988 , vol. 29, # 17 p. 2033 - 2036
反应条件
nitric acid; acetic anhydride in dichloromethane T=-20°C;
参考文献
Bushnell, Gordon W.; Fischer, Alfred; Ibrahim, Prabha N.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1281 - 1286
反应条件
in dichloromethane T=-40 - 20°C; 8 h;
参考文献
Page, T. Keri; Wirth, Thomas
Synthesis, 2006 , # 18 p. 3153 - 3155
反应条件
in dichloromethane Ambient temperature;
参考文献
Zefirov, N. S.; Safronov, S. O.; Kaznacheev, A. A.; Zhdankin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 8.2 p. 1633 - 1634
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 8 p. 1807 - 1808
反应条件
1: 88.8 percent / acetic acid, H2O2, H2SO4 / H2O / 1.) 29-31 deg C, 65 min; 2.) 0 deg C, 75 min 2: 78.5 percent / 50 - 55 °C View Scheme
参考文献
Saginova. L. G.; Bondarenko, O. B.; Shabarov, Yu. S.; Gazzaev, R. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1935 - 1939
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2124 - 2129
反应条件
trifluoroacetic anhydride in chloroform
参考文献
Szantay, Csaba; Blasko, Gabor; Barczai-Beke, Marietta; Pechy, Peter; Dornyei, Gabor
Tetrahedron Letters, 1980 , vol. 21, p. 3509 - 3512
反应条件
1: (bistrifluoroacetoxyiodo)benzene / nitromethane / 1 h / 20 °C 2: 30percent H2O2 View Scheme
参考文献
Saginova. L. G.; Bondarenko, O. B.; Shabarov, Yu. S.; Gazzaev, R. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1935 - 1939
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2124 - 2129