[双(三氟乙酰氧基)碘]苯合成路线 （共 95 条）
反应条件
iodine in dichloromethane; ethyl acetate
参考文献
Bristol-Myers Squibb Company
Patent: US2011/263494 A1, 2011 ;
US 20110263494 A1
反应条件
1: 70 percent / acetonitrile / 72 h / Ambient temperature
2: HCl gas
3: 35 percent / NaN3 / dimethylformamide / 0.08 h / 60 °C
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
反应条件
1: 70 percent / acetonitrile / 72 h / Ambient temperature
2: HCl gas
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
反应条件
1: 70 percent / acetonitrile / 72 h / Ambient temperature
2: 0.17 h
View Scheme
参考文献
Spyroudis, Spyros; Varvoglis, Anastasios
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 135 - 137
反应条件
in dichloromethane
10 h; Ambient temperature;
参考文献
Macdonald, Timothy L.; Narasimhan, Narayanan
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 5000 - 5001
反应条件
iodine in chloroform; trifluoroacetic acid
T=-30°C; 5 h; Product distribution;
参考文献
Saginova. L. G.; Bondarenko, O. B.; Shabarov, Yu. S.; Gazzaev, R. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 1935 - 1939
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 10 p. 2124 - 2129
反应条件
in dichloromethane
17 h; Ambient temperature;
参考文献
Boyer, Joseph H.; Natesh, Anbazhagan
Synthesis, 1988 , # 12 p. 980 - 981
反应条件
in chloroform
T=20°C; 24 h;
参考文献
Barbas, Dimitris; Spyroudis, Spyros; Varvoglis, Anastasios
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2201 - 2214
反应条件
in chloroform
T=20°C; 24 h;
参考文献
Barbas, Dimitris; Spyroudis, Spyros; Varvoglis, Anastasios
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2201 - 2214
反应条件
in chloroform
T=20°C; 24 h;
参考文献
Barbas, Dimitris; Spyroudis, Spyros; Varvoglis, Anastasios
Journal of Chemical Research, Miniprint, 1985 , # 6 p. 2201 - 2214
