N-苄基-2-氟苯基甘氨酸合成路线 （共 5 条）
反应条件
sodium hydroxide; hydrazine hydrate; palladium on activated charcoal in water Hydrogenolysis; 10 h; Heating;
参考文献
Davies, Antony J.; Ashwood, Michael S.; Cottrell, Ian F.
Synthetic Communications, 2000 , vol. 30, # 6 p. 1095 - 1102
反应条件
sodium hydroxide; water in various solvent(s)
Hydrolysis; 3.5 h; Heating;
参考文献
Davies, Antony J.; Ashwood, Michael S.; Cottrell, Ian F.
Synthetic Communications, 2000 , vol. 30, # 6 p. 1095 - 1102
反应条件
1: Na2S2O5 / methanol; H2O / 2 h / 35 °C
2: 85 percent / aq. H2O2; K2CO3 / dimethylsulfoxide / 16.5 h / 21 - 35 °C
3: 86 percent / NaOH; H2O / various solvent(s) / 3.5 h / Heating
View Scheme
参考文献
Davies, Antony J.; Ashwood, Michael S.; Cottrell, Ian F.
Synthetic Communications, 2000 , vol. 30, # 6 p. 1095 - 1102
反应条件
1: 85 percent / aq. H2O2; K2CO3 / dimethylsulfoxide / 16.5 h / 21 - 35 °C
2: 86 percent / NaOH; H2O / various solvent(s) / 3.5 h / Heating
View Scheme
参考文献
Davies, Antony J.; Ashwood, Michael S.; Cottrell, Ian F.
Synthetic Communications, 2000 , vol. 30, # 6 p. 1095 - 1102
反应条件
1: Na2S2O5 / methanol; H2O / 2 h / 35 °C
2: 85 percent / aq. H2O2; K2CO3 / dimethylsulfoxide / 16.5 h / 21 - 35 °C
3: 86 percent / NaOH; H2O / various solvent(s) / 3.5 h / Heating
View Scheme
参考文献
Davies, Antony J.; Ashwood, Michael S.; Cottrell, Ian F.
Synthetic Communications, 2000 , vol. 30, # 6 p. 1095 - 1102
