diphenyl-phenyl carbinol; trifluoroacetic acid 48 h; Heating;

(i) SOCl2, Py, Et2O, (ii) SnCl4, benzene, (iii) aq. HCl; Multistep reaction;

暂无反应条件数据

2: palladium coal / 300 - 320 °C View Scheme

1: NaBH4 / tetrahydrofuran; methanol / 4.5 h 2: tosic acid / benzene / 1 h / Heating 3: 80 percent / I2 / benzene / 4 h / Heating 4: 2.97 g / p-toluenesulfonic acid / benzene / 24 h / Heating 5: 71 percent / DDQ / benzene 6: 85 percent / glacial acetic acid, concd. HCl / 24 h / Heating View Scheme

1: NaBH4 / tetrahydrofuran; methanol / 4.5 h 2: tosic acid / benzene / 1 h / Heating 3: 80 percent / I2 / benzene / 4 h / Heating 4: 2.97 g / p-toluenesulfonic acid / benzene / 24 h / Heating 5: 71 percent / DDQ / benzene 6: 85 percent / glacial acetic acid, concd. HCl / 24 h / Heating 7: 82 percent / Adogen 464, Fremy's salt, KH2PO4 / H2O / 1 h View Scheme

1: NaBH4 / tetrahydrofuran; methanol / 4.5 h 2: tosic acid / benzene / 1 h / Heating 3: 80 percent / I2 / benzene / 4 h / Heating 4: 2.97 g / p-toluenesulfonic acid / benzene / 24 h / Heating 5: 71 percent / DDQ / benzene 6: 85 percent / glacial acetic acid, concd. HCl / 24 h / Heating 7: 82 percent / Adogen 464, Fremy's salt, KH2PO4 / H2O / 1 h 8: 91 percent / NaBH4, O2 / ethanol / 28 h 9: 61 percent / N-bromosuccinimide / dimethylsulfoxide; H2O / 1 h / Ambient temperature 10: 76 percent / potasium tert-butoxide / tetrahydrofuran; 2-methyl-propan-2-ol / 0.5 h / Ambient temperature View Scheme