反应条件
1: NH2OH*HCl
2: 1.) 15percent n-BuLi, (i-Pr)2NH / 1.) THF, hexane, -75 deg C, 30 min, 2.) -75 deg C, 1 h; up to r.t., 2 h
3: 1.) 15percent n-BuLi / 1.) THF, hexane, -75 deg C, 30 min, 2.) -75 deg C, 1 h; up to r.t., 2 h
4: 1M HCl / diethyl ether / Ambient temperature
View Scheme
参考文献
Konakahara, Takeo; Kurosaki, Yoshihiro
Journal of Chemical Research, Miniprint, 1989 , # 5 p. 1068 - 1086
