2-乙基-3-甲基-喹啉合成路线 （共 54 条）
反应条件
1 wt Pt on TiO2
T=120°C; P=3800.26 Torr; 8 h; AutoclaveInert atmosphere;
参考文献
He, Lin; Wang, Jian-Qiang; Gong, Ya; Liu, Yong-Mei; Cao, Yong; He, He-Yong; Fan, Kang-Nian
Angewandte Chemie - International Edition, 2011 , vol. 50, # 43 p. 10216 - 10220
反应条件
1: 1 Au/TiO2 / 8 h / 120 °C / 3800.26 Torr / Autoclave; Inert atmosphere
2: titania-supported iridium nanoclusters / tert-butyl alcohol / 8 h / 120 °C / 3800.26 Torr / Autoclave; Inert atmosphere
View Scheme
参考文献
He, Lin; Wang, Jian-Qiang; Gong, Ya; Liu, Yong-Mei; Cao, Yong; He, He-Yong; Fan, Kang-Nian
Angewandte Chemie - International Edition, 2011 , vol. 50, # 43 p. 10216 - 10220
反应条件
1: With trifluorormethanesulfonic acid in chloroform-d1
T=-30°C; Friedlaender-Borsche synthesis;
2: in chloroform-d1
T=50°C; Friedlaender-Borsche synthesis;
3: With sodium hydroxide in chloroform-d1; water
参考文献
Vicente, Jose; Chicote, Maria Teresa; Martinez-Martinez, Antonio Jesus
Tetrahedron Letters, 2011 , vol. 52, # 47 p. 6298 - 6302
反应条件
tetrachloromethane; [Ni(O2CCH3)2]*4H2O; triethylamine
T=135 - 145°C; 16 h; Inert atmosphere;
参考文献
Khusnutdinov; Baygusina; Aminov; Dzhemilev
Russian Journal of Organic Chemistry, 2012 , vol. 48, # 5 p. 690 - 693
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; tin(ll) chloride in 1,4-dioxane; water
T=180°C; Alkylation; cyclocondensation; 20 h; Product distribution; Further Variations:ReagentsSolventsreaction times;
参考文献
Cho, Chan Sik; Kim, Joon Seok; Oh, Byoung Ho; Kim, Tae-Jeong; Shim, Sang Chul; Yoon, Nam Sik
Tetrahedron, 2000 , vol. 56, # 39 p. 7747 - 7750
反应条件
10 palladium on activated charcoal; palladium dichloride in acetonitrile
T=80°C; 48 h;
参考文献
Matsubara, Yoshio; Hirakawa, Saori; Yamaguchi, Yoshihiro; Yoshida, Zen-Ichi
Angewandte Chemie - International Edition, 2011 , vol. 50, # 33 p. 7670 - 7673
反应条件
titania-supported iridium nanoclusters
T=120°C; P=3800.26 Torr; 8 h; AutoclaveInert atmosphere;
参考文献
He, Lin; Wang, Jian-Qiang; Gong, Ya; Liu, Yong-Mei; Cao, Yong; He, He-Yong; Fan, Kang-Nian
Angewandte Chemie - International Edition, 2011 , vol. 50, # 43 p. 10216 - 10220
反应条件
1: Pb(OCOCH3)4
2: 1.) pyrrolidine, p-TsOH, 2.) ZnBr2 / 1.) benzene, 10 h, 2.) chloroform, 90 deg C-100 deg C, 10 h
View Scheme
参考文献
Koyama, Junko; Toyokuni, Izumi; Tagahara, Kiyoshi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 2 p. 332 - 334
反应条件
1: sec-BuLi / tetrahydrofuran; hexane / 1.) 0 deg C, 2 h, 2.) 0 deg C, 1 h; r.t., 12 h
2: KHMDS / tetrahydrofuran; hexane; toluene / 2 h / Ambient temperature
View Scheme
参考文献
Ubeda, J. Ignacio; Villacampa, Mercedes; Avendano, Carmen
Synthesis, 1998 , # 8 p. 1176 - 1180
反应条件
titania-supported iridium nanoclusters
T=180°C; P=3800.26 Torr; 1.2 h; AutoclaveInert atmosphere;
参考文献
He, Lin; Wang, Jian-Qiang; Gong, Ya; Liu, Yong-Mei; Cao, Yong; He, He-Yong; Fan, Kang-Nian
Angewandte Chemie - International Edition, 2011 , vol. 50, # 43 p. 10216 - 10220
