2,2-二硝基丙烷-1,3-二醇合成路线 （共 21 条）
参考文献
Feuer et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 1360
反应条件
acetic acid; 1-n-butyl-3-methylimidazolium tetrafluoroborate
T=1 - 3°C;
参考文献
Epishina, Margarita A.; Ovchinnikov, Igor V.; Kulikov, Alexander S.; Makhova, Nina N.; Tartakovsky, Vladimir A.
Mendeleev Communications, 2011 , vol. 21, # 1 p. 21 - 23
反应条件
sodium hydroxide; silver nitrate; sodium nitrite
参考文献
Borgardt,F.G. et al.
Journal of Organic Chemistry, 1966 , vol. 31, p. 2806 - 2811
反应条件
in diethyl ether; water
T=18 - 25°C; 120 h;
参考文献
Nekrasova, G. V.; Lipina, E. S.; Zagibalova, L. Ya.; Perekalin, V. V.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 4 p. 619 - 623
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 4 p. 711 - 716
反应条件
formaldehyd
with 30percent formaldehyde in reflux 500-600 h;
参考文献
Gmelin Handbook: F: PerFHalOrg.8, 2.4, page 2 - 54
参考文献
Fridman,A.L. et al.
Journal of Organic Chemistry USSR (English Translation), 1967 , vol. 3, p. 1485 - 1486
Zhurnal Organicheskoi Khimii, 1967 , vol. 3, p. 1529 - 1530
Full Text Show Details
Fridman,A.L. et al.
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 980 - 985,966 - 970
参考文献
Fridman,A.L. et al.
Zhurnal Organicheskoi Khimii, 1969 , vol. 5, p. 980 - 985,966 - 970
反应条件
1: With potassium amidosulfonate in ethanol; water
Condensation; Cyclization; pH=4.7;
2: With sulfuric acid; nitric acid in water
T=-15 - -10°C; Nitration; 0.5 h;
参考文献
Tartakovsky; Ermakov; Varfolomeeva
Russian Chemical Bulletin, 1999 , vol. 48, # 7 p. 1385 - 1387
反应条件
sulfuric acid; acetic acid
参考文献
Gold et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1665
参考文献
Gold et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1665
