1: 1-phenyl-5-(prop-2'-ene-1'-sulfonyl)-1H-tetrazole With potassium hexamethylsilazane in ethylene glycol dimethyl ether
T=-60°C; Metallation; 0.5 h;
2: Decanaldehyde T=-60 - 20°C; Julia olefination; Title compound not separated from byproducts;
参考文献
Kocienski, Philip J.; Bell, Alan; Blakemore, Paul R.
Synlett, 2000 , # 3 p. 365 - 366