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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
奥苷菊环
合成路线
（共 184 条）
586-78-7
1-溴-4-硝基苯
+
441292-61-1
→
反应条件
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1,4-dioxane 2 h; Heating;
参考文献
Okujima, Tetsuo; Ito, Shunji; Morita, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1261 - 1264
106-38-7
对溴甲苯
+
35046-05-0
→
反应条件
73393-11-0
+
102435-38-1
+
275-51-4
奥苷菊环
反应条件
1: 6-bromoazulene With 1,1,1,2,2,2-hexabutyl-distannane; tetrakis(triphenylphosphine) palladium(0) in toluene 24 h; Heating; 2: para-bromotoluene With tri-tert-butyl phosphine; cesium fluoride; tris(dibenzylideneacetone)dipalladium (0) in 1,4-dioxane Stille cross-coupling; 24 h; Heating; Further stages.;
参考文献
Ito, Shunji; Okujima, Tetsuo; Morita, Noboru
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 16 p. 1896 - 1905
106-43-4
对氯甲苯
+
457644-50-7
→
反应条件
82893-99-0
+
111679-38-0
+
275-51-4
奥苷菊环
反应条件
barium dihydroxide; Cs2C03; tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine in 1,4-dioxane T=80°C; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
106-37-6
对二溴苯
+
457644-50-7
→
反应条件
19227-07-7
2-苯基-薁
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
626-39-1
1,3,5-三溴苯
+
457644-50-7
→
反应条件
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
457644-50-7
+
583-53-9
1,2-二溴苯
→
反应条件
19227-07-7
2-苯基-薁
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; caesium carbonate in 1,4-dioxane T=80°C; Miyaura-Suzuki cross-coupling; 24 h;
参考文献
Ito, Shunji; Terazono, Tomomi; Kubo, Takahiro; Okujima, Tetsuo; Morita, Noboru; Murafuji, Toshihiro; Sugihara, Yoshikazu; Fujimori, Kunihide; Kawakami, Jun; Tajiri, Akio
Tetrahedron, 2004 , vol. 60, # 25 p. 5357 - 5366
19384-00-0
2-薁并l
→
反应条件
275-51-4
奥苷菊环
反应条件
1: 95 percent / Et3N / CH2Cl2 / 0.5 h / 20 °C 2: 96 percent / HCOOH; P(o-tolyl)3; n-Bu3N / Pd2(dba)3 / dioxane / 24 h / Heating View Scheme
参考文献
Ito, Shunji; Yokoyama, Ryuji; Okujima, Tetsuo; Terazono, Tomomi; Kubo, Takahiro; Tajiri, Akio; Watanabe, Masataka; Morita, Noboru
Organic and biomolecular chemistry, 2003 , vol. 1, # 11 p. 1947 - 1952
17975-54-1
→
反应条件
91-20-3
萘
+
1608-03-3
+
935-01-3
+
275-51-4
奥苷菊环
反应条件
T=680 - 750°C; P=0.001 - 0.1 Torr; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Becker, Juergen; Wentrup, Curt; Katz, Ellen; Zeller, Klaus-Peter
Journal of the American Chemical Society, 1980 , vol. 102, # 15 p. 5110 - 5112
104-92-7
4-溴苯甲醚
+
441292-61-1
→
反应条件
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1,4-dioxane 6 h; Heating;
参考文献
Okujima, Tetsuo; Ito, Shunji; Morita, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1261 - 1264
106-38-7
对溴甲苯
+
441292-61-1
→
反应条件
73393-11-0
+
102435-38-1
+
275-51-4
奥苷菊环
反应条件
tris(dibenzylideneacetone)dipalladium (0); tri-tert-butyl phosphine; cesium fluoride in 1,4-dioxane 24 h; Heating;
参考文献
Okujima, Tetsuo; Ito, Shunji; Morita, Noboru
Tetrahedron Letters, 2002 , vol. 43, # 7 p. 1261 - 1264
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