3-甲基-2-环戊烯-1-酮合成路线 (共 109 条)
反应条件
hydrogenchloride; hydrogen sulfide
参考文献
Metzner,P.; Vialle,J.
Bulletin de la Societe Chimique de France, 1972 , p. 3138 - 3145
反应条件
hydrogen; HRuCl(TBPC)2 in benzene T=80°C; P=30400 Torr; 8 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Massonneau, Viviane; Maux, Paul Le; Simonneaux, Gerard
Journal of Organometallic Chemistry, 1987 , vol. 327, p. 269 - 274
反应条件
sodium tetrahydroborate in methanol T=20°C; 0.333333 h; Inert atmosphere;
参考文献
Forkel, Nina V.; Henderson, David A.; Fuchter, Matthew J.
Green Chemistry, 2012 , vol. 14, # 8 p. 2129 - 2132
反应条件
1: H2O2; H2O; NaOH / methanol / 0 °C 2: 74 percent / LiClO4 / diethyl ether / 6 h / 20 °C View Scheme
参考文献
Ho, Tse-Lok; Lui, Shing-Hou
Synthetic Communications, 1983 , vol. 13, # 8 p. 685 - 690
反应条件
1: 22 percent 2: 84 percent / zeolite beta according Wadlinger; 1,3,5-tri(tert-butyl)benzene / benzene / 3 h / Heating View Scheme
参考文献
European Journal of Organic Chemistry, , # 10 p. 1905 - 1911
反应条件
sodium hydroxide in 1,4-dioxane; water 7 h; Reflux;
参考文献
Pourali, Ali Reza
Mendeleev Communications, 2010 , vol. 20, # 2 p. 113 - 115
反应条件
sodium hydroxide in dichloromethane; dihydrogen peroxide
参考文献
SCM Corporation
Patent: US4359586 A1, 1982 ;
反应条件
hydrogenchloride; ammonium chloride in diethyl ether; water
参考文献
Mitsui Chemicals, Inc.
Patent: EP1138687 A1, 2001 ;
反应条件
nickel dichloride; zinc in 2-methoxy-ethanol; water T=30°C; 1 h; ultrasonic irradiation;
参考文献
Petrier, Christian; Luche, Jean-Louis
Tetrahedron Letters, 1987 , vol. 28, # 21 p. 2347 - 2350
反应条件
manganese triacetate in benzene 8 h; Heating;
参考文献
Tanyeli, Cihangir; Oezdemirhan, Devrim
Tetrahedron Letters, 2002 , vol. 43, # 22 p. 3977 - 3980