2,5-脱水-D-葡萄糖醇合成路线 （共 29 条）
反应条件
palladium on activated charcoal; hydrogen; acetic acid in methanol
参考文献
Aragao-Leoneti, Valquiria; Carvalho, Ivone
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1087 - 1089
反应条件
sodium methylate in methanol 25 h;
参考文献
Kuszmann, Janos; Dvortsak, Peter
Carbohydrate Research, 1983 , vol. 123, p. 209 - 230
反应条件
hydrogen bromide in acetic acid T=0°C;
参考文献
Rolf; Gray
Carbohydrate research, 1984 , vol. 131, # 1 p. 17 - 28
反应条件
1: 84 percent / OsO4; CSA; Me3NO / CH2Cl2 2: 99 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Donohoe, Timothy J.; Butterworth, Sam
Angewandte Chemie - International Edition, 2003 , vol. 42, # 8 p. 948 - 951
反应条件
sodium tetrahydroborate in water 24 h;
参考文献
Bendiak, Brad; Salayan, Mary E.; Pantoja, Mario
Journal of Organic Chemistry, 1995 , vol. 60, # 25 p. 8245 - 8256
反应条件
toluene-4-sulfonic acid T=180°C; Reagent/catalyst;
参考文献
ARCHER DANIELS MIDLAND COMPANY; BINDER, Thomas P.; SANBORN, Alexandra
Patent: WO2013/138153 A1, 2013 ;
Location in patent: Paragraph 00129-00130 ;
反应条件
sodium methylate in methanol 48 h; Ambient temperature;
参考文献
Kuszmann, Janos; Dvortsak, Peter
Carbohydrate Research, 1983 , vol. 123, p. 209 - 230
反应条件
1.1: 4-methylmorpholine N-oxide; OsO4 / tetrahydrofuran; H2O / 20 °C 1.2: 48 percent / NaIO4 / methanol; tetrahydrofuran; H2O / 2 h / 20 °C 2.1: 92 percent / NaBH4 / ethanol / 2 h 3.1: 61 percent / H2 / Pd/C / methanol / 18 h / 20 °C View Scheme
参考文献
Persky, Rachel; Albeck, Amnon
Journal of Organic Chemistry, 2000 , vol. 65, # 18 p. 5632 - 5638
反应条件
Sn-Beta zeolite in water T=109.84°C; 1 h;
参考文献
Moliner, Manuel; Roman-Leshkov, Yuriy; Davis, Mark E.
Proceedings of the National Academy of Sciences of the United States of America, 2010 , vol. 107, # 14 p. 6164 - 6168
反应条件
Ti-Beta zeolite in water T=109.84°C; 1.5 h;
参考文献
Moliner, Manuel; Roman-Leshkov, Yuriy; Davis, Mark E.
Proceedings of the National Academy of Sciences of the United States of America, 2010 , vol. 107, # 14 p. 6164 - 6168
