环己基-(4-甲基苯基)甲酮合成路线 （共 14 条）
反应条件
1: para-bromotoluene With magnesium in tetrahydrofuran
T=20°C; 1 h;
2: cyclohexanecarbaldehyde in tetrahydrofuran
T=0 - 20°C; 2 h;
3: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrahydrofuran; tert-butyl alcohol
20 h; RefluxDarkness;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 32 p. 6557 - 6564
反应条件
1: 1-bromocyclohexane With magnesium in tetrahydrofuran
T=20°C; 1 h;
2: 4-methyl-benzaldehyde in tetrahydrofuran
T=0 - 20°C; 2 h;
3: With 1,3-Diiodo-5,5-dimethyl-2,4-imidazolidinedione; potassium carbonate in tetrahydrofuran; tert-butyl alcohol
23 h; RefluxDarkness;
参考文献
Dohi, Souya; Moriyama, Katsuhiko; Togo, Hideo
Tetrahedron, 2012 , vol. 68, # 32 p. 6557 - 6564
反应条件
triethylamine; triphenylphosphine; palladium dichloride in 1,4-dioxane
T=80°C; 4 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Jadhav, Deepak N.
Tetrahedron Letters, 2006 , vol. 47, # 39 p. 6975 - 6978
反应条件
carbon monoxide; tri-ruthenium(0)dodecacarbonyl
T=200°C; P=14710.2 Torr; 48 h;
参考文献
Kondo, Teruyuki; Tsui, Yasushi; Watanabe, Yoshihisa
Tetrahedron Letters, 1987 , vol. 28, # 49 p. 6229 - 6230
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran
T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran
T=55°C; 16 h;
参考文献
Fausett, Bryan W.; Liebeskind, Lanny S.
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4851 - 4853
反应条件
bis(1,5-cyclooctadiene)nickel (0); bathophenanthroline; magnesium chloride; zinc in acetonitrile
T=25°C; 12 h; Inert atmosphere;
参考文献
Yin, Hongyu; Zhao, Chenglong; You, Hengzhi; Lin, Kunhua; Gong, Hegui
Chemical Communications, 2012 , vol. 48, # 56 p. 7034 - 7036
反应条件
diethyl ether
T=135 - 145°C; Erhitzen des Reaktionsprodukts mit KHSO4;
参考文献
English et al.
Journal of the American Chemical Society, 1950 , vol. 72, p. 1653
反应条件
in diethyl ether
T=-78 - 25°C;
参考文献
Dar; Thiruvazhi; Abraham; Kitayama; Kopajtic; Gamliel; Slusher; Carroll; Uhl
European Journal of Medicinal Chemistry, 2005 , vol. 40, # 10 p. 1013 - 1021
反应条件
aluminium trichloride
参考文献
Coleman,J.P. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1970 , p. 666 - 670
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Henze; Isbell
Journal of the American Chemical Society, 1954 , vol. 76, p. 4152,4154
