1,1,1-三(4-羟基苯基)乙烷合成路线 （共 9 条）
反应条件
methanesulfonic acid; 3-mercapto-propionic acid T=55°C; 20.5 h; Product distribution / selectivity;
参考文献
Kishan, Gurram; Ramanarayanan, G.V.; Ravindra, Khanwelkar Rahul; Dhalla, Adil Minoo; Rai, Vinod Kumar; Kulkarni, Surendra Umesh
Patent: US2006/4214 A1, 2006 ;
Location in patent: Page/Page column 4-5 ;
反应条件
MPS; ion exchange resin A-121 (manufactured by Rohm Haas) T=75°C; 22 h;
参考文献
Dhalla, Adil Minoo; Gupta, Raina; Kishan, Gurram; Li, Yongcheng; Ramanarayanan, G.V.
Patent: US2006/173222 A1, 2006 ;
Location in patent: Page/Page column 5-7 ;
反应条件
ethyl mercaptan sodium salt in N,N-dimethyl-formamide
参考文献
O'Krongly, David; Denmeade, Samuel R.; Chiang, Michael Y.; Breslow, Ronald
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5544 - 5545
反应条件
2: NaSEt / dimethylformamide View Scheme
参考文献
O'Krongly, David; Denmeade, Samuel R.; Chiang, Michael Y.; Breslow, Ronald
Journal of the American Chemical Society, 1985 , vol. 107, # 19 p. 5544 - 5545
参考文献
Dhalla, Adil Minoo; Gupta, Raina; Kishan, Gurram; Li, Yongcheng; Ramanarayanan, G.V.
Patent: US2006/173222 A1, 2006 ;
Location in patent: Page/Page column 6 ;
反应条件
methanesulfonic acid; 3-mercapto-propionic acid T=35 - 55°C; 22 h; Product distribution / selectivity;
参考文献
Kishan, Gurram; Ramanarayanan, G.V.; Ravindra, Khanwelkar Rahul; Dhalla, Adil Minoo; Rai, Vinod Kumar; Kulkarni, Surendra Umesh
Patent: US2006/4214 A1, 2006 ;
Location in patent: Page/Page column 5 ;
参考文献
Nowakowska, Ewa; Daszkiewicz, Zdzislaw; Kyziol, Janusz B.
Tetrahedron Letters, 1998 , vol. 39, # 5-6 p. 451 - 454
反应条件
in tetrachloromethane T=24.84°C; Equilibrium constant;
参考文献
Hunter, Christopher A.; Ihekwaba, Ndidi; Misuraca, Maria Cristina; Segarra-Maset, Maria Dolores; Turega, Simon M.
Chemical Communications, 2009 , # 26 p. 3964 - 3966
反应条件
potassium carbonate in N,N-dimethyl-formamide T=130°C; 12 h;
参考文献
Shiina, Yoshikatsu; Morikawa, Atsushi
Reactive and Functional Polymers, 2011 , vol. 71, # 2 p. 85 - 94
