2’-羟基-4-氯苯乙酮合成路线 （共 36 条）
反应条件
hydrogenchloride; potassium hydroxide; iodobenzene diacetate in methanol; ethanol; water
参考文献
Rohm and Haas Company
Patent: US5552409 A1, 1996 ;
反应条件
water; barium carbonate
参考文献
Lee; Jin; Choi
Chemical Communications, 2001 , # 11 p. 956 - 957
反应条件
water T=100°C; 0.416667 h;
参考文献
Utsukihara, Takamitsu; Nakamura, Hiroaki; Watanabe, Masashige; Akira Horiuchi
Tetrahedron Letters, 2006 , vol. 47, # 52 p. 9359 - 9364
反应条件
iodosylbenzene; boron trifluoride diethyl etherate; water in dichloromethane 1.) -40 deg C, 1 h, 2.) room temp., 30 min;
参考文献
Moriarty, Robert M.; Prakash, Om; Duncan, Michael P.
Synthesis, 1985 , # 10 p. 943 - 944
反应条件
1: With tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide in dichloromethane T=20°C; 3 h; 2: With Oxonereg; in methanol; water T=20°C; 3 h;
参考文献
Tsujigami, Toshikuni; Sugai, Takeshi; Ohta, Hiromichi
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2543 - 2549
反应条件
in methanol T=25°C; Kinetics; Concentration;
参考文献
Tagawa, Kohei; Sasagawa, Keita; Wakisaka, Ken; Monjiyama, Shunsuke; Katayama, Mika; Yamataka, Hiroshi
Bulletin of the Chemical Society of Japan, 2014 , vol. 87, # 1 p. 119 - 126
反应条件
1: 96 percent / CH2Cl2 / 0.75 h / 20 °C 2: 89 percent / Et3N / CH2Cl2; methanol / 12 h / 20 °C View Scheme
参考文献
Craig, Donald; Daniels, Kevin; MacKenzie, A. Roderick
Tetrahedron Letters, 1990 , vol. 31, # 44 p. 6441 - 6444
反应条件
in methanol T=25°C; Kinetics; Concentration;
参考文献
Tagawa, Kohei; Sasagawa, Keita; Wakisaka, Ken; Monjiyama, Shunsuke; Katayama, Mika; Yamataka, Hiroshi
Bulletin of the Chemical Society of Japan, 2014 , vol. 87, # 1 p. 119 - 126
反应条件
in acetone T=25°C; 3 h;
参考文献
Kovac, F.; Baumstark, A. L.
Tetrahedron Letters, 1994 , vol. 35, # 47 p. 8751 - 8754
反应条件
1.1: m-CPBA / CHCl3 / 20 °C 1.2: 23 percent / sulfuric acid / CHCl3; H2O / 1 h / 20 °C 2.1: 4-dimethylaminopyridine; triethylamine / CH2Cl2 / 20 °C 3.1: tetrapropylammonium perruthenate; N-methylmorpholine N-oxide / CH2Cl2 / 3 h / 20 °C 3.2: 183 mg / Oxone / H2O; methanol / 3 h / 20 °C View Scheme
参考文献
Tsujigami, Toshikuni; Sugai, Takeshi; Ohta, Hiromichi
Tetrahedron Asymmetry, 2001 , vol. 12, # 18 p. 2543 - 2549
