反应条件
in neat (no solvent)
decompn. on storing at 20°C (several h, Ar);; condensation into a cooled trap (-78°C, E-4 Torr); contaminated,purity: 85percent;;
参考文献
Poerschke, Klaus-Richard; Wilke, Guenther; Mynott, Richard
Chemische Berichte, 1985 , vol. 118, # 1 p. 298 - 312
