1-环状己烯三氟甲烷磺酸合成路线 （共 56 条）
反应条件
1: 3-Fluorophenylmagnesium bromide With zinc dibromide in tetrahydrofuran T=20°C; 2: carbon monoxide; cyclohex-1-en-1-yl trifluoromethanesulfonate With magnesium bromide; nickel dichloride in tetrahydrofuran; dimethyl sulfoxide T=50°C; Negishi coupling; P=760.051 Torr; 0.333333 h; Further stages.;
参考文献
Wang, Qiaoling; Chen, Chuo
Tetrahedron Letters, 2008 , vol. 49, # 18 p. 2916 - 2921
反应条件
lutidine; water in ethanol T=125.2 - 175.5°C; Kinetics;
参考文献
Pfeifer,W.D. et al.
Journal of the American Chemical Society, 1971 , vol. 93, # 6 p. 1513 - 1516
反应条件
tetraethylammonium bromide; triethylamine T=135°C; 360 h; Product distributionMechanism;
参考文献
Chemische Berichte, , vol. 117, # 9 p. 2815 - 2824
反应条件
1: 2-propen-2-ylmagnesium bromide With zinc dibromide in tetrahydrofuran T=20°C; 2: carbon monoxide; cyclohex-1-en-1-yl trifluoromethanesulfonate With magnesium bromide; nickel dichloride in tetrahydrofuran; dimethyl sulfoxide T=50°C; Negishi coupling; P=760.051 Torr; 0.533333 h; Further stages.;
参考文献
Wang, Qiaoling; Chen, Chuo
Tetrahedron Letters, 2008 , vol. 49, # 18 p. 2916 - 2921
反应条件
bis (triortho-tolylphosphine)palladium(II) chloride in tetrahydrofuran Ambient temperature;
参考文献
Nakamura, Eiichi; Aoki, Satoshi; Sekiya, Kouichi; Oshino, Hiroji; Kuwajima, Isao
Journal of the American Chemical Society, 1987 , vol. 109, # 26 p. 8056 - 8066
反应条件
1-methyl-pyrrolidin-2-one; iron (III) acetylacetonate in tetrahydrofuran T=-30°C;
参考文献
Scheiper, Bodo; Bonnekessel, Melanie; Krause, Helga; Fuerstner, Alois
Journal of Organic Chemistry, 2004 , vol. 69, # 11 p. 3943 - 3949
反应条件
tris(4-methoxyphenyl)-phosphine; Co(acetylacetonate)3 in tetrahydrofuran T=20°C; 3 h;
参考文献
Shirakawa, Eiji; Imazaki, Yusuke; Hayashi, Tamio
Chemistry Letters, 2008 , vol. 37, # 6 p. 654 - 655
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate; triphenylphosphine in N,N-dimethyl acetamide T=55°C; P=1551.49 Torr; 16 h; regioselective reaction;
参考文献
Saini, Vaneet; Sigman, Matthew S.
Journal of the American Chemical Society, 2012 , vol. 134, # 28 p. 11372 - 11375
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium tert-butylate in N,N-dimethyl acetamide T=55°C; 24 h;
参考文献
Liao, Longyan; Jana, Ranjan; Urkalan, Kaveri Balan; Sigman, Matthew S.
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5784 - 5787
反应条件
potassium fluoride; tris-(dibenzylideneacetone)dipalladium(0) in N,N-dimethyl acetamide T=20°C; 12 h;
参考文献
Liao, Longyan; Jana, Ranjan; Urkalan, Kaveri Balan; Sigman, Matthew S.
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5784 - 5787
