N,N'-1,2-乙烷二基二[N-[2-[(二乙氧基亚膦酰)氨基]乙基]-氨基磷酸 P,P,P',P'-四乙基酯合成路线 （共 2 条）
反应条件
tetrachloromethane; sodium hydrogencarbonate; potassium carbonate; tetrabutylammomium bromide in dichloromethane T=0 - 20°C;
参考文献
Gray Jr., Charles W.; Barry, Kathleen; Lindberg, Eric J.; Houston, Todd A.
Tetrahedron Letters, 2007 , vol. 48, # 15 p. 2683 - 2686
反应条件
1: 80 percent / Bu4N(HSO4); aq. 50 percent NaOH / toluene / 4 h / Heating
2: 86 percent / HCl gas; NaOH / dioxane / 20 °C
View Scheme
参考文献
Chellini, Andrea; Pagliarin, Roberto; Giovenzanna, Giovanni B.; Palmisano, Giovanni; Sisti, Massimo
Helvetica Chimica Acta, 2000 , vol. 83, # 4 p. 793 - 800
