3,4-(亚甲基二氧)苯丙酮合成路线 （共 32 条）
反应条件
[bis(acetoxy)iodo]benzene in dichloromethane T=50°C; 0.0833333 h; Microwave irradiation; TimeTemperatureSolvent;
参考文献
Alvarez, Heiddy Marquez; Barbosa, Dayse P.; Fricks, Alini Tinoco; Aranda, Donato A. G.; Valdes, Ricardo H.; Antunes
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 941 - 943
反应条件
PhI(OAc)2/Al2O3 T=140°C; 0.5 h; Microwave irradiation;
参考文献
Alvarez, Heiddy Marquez; Barbosa, Dayse P.; Fricks, Alini Tinoco; Aranda, Donato A. G.; Valdes, Ricardo H.; Antunes
Organic Process Research and Development, 2006 , vol. 10, # 5 p. 941 - 943
反应条件
hydrogenchloride; water in diethyl ether T=20°C; 1 h; Inert atmosphere;
参考文献
Ruan, Jiwu; Iggo, Jonathan A.; Berry, Neil G.; Xiao, Jianliang
Journal of the American Chemical Society, 2010 , vol. 132, # 46 p. 16689 - 16699
反应条件
potassium hydroxide; dichloromethane T=120°C;
参考文献
Winthrop Chem. Co.
Patent: US1964973 , 1932 ;
反应条件
diethyl ether; ethylmagnesium bromide Erwaermen des erhaltenen 1-Benzo<1,3>dioxol-5-yl-propan-1-on-imins mit wss. Salzsaeure;
参考文献
Fuson; Gaertner; Chadwick
Journal of Organic Chemistry, 1948 , vol. 13, p. 489,493
反应条件
potassium permanganate sonication;
参考文献
Kumar, Vinod; Sharma, Abhishek; Sharma, Meenakshi; Sharma, Upendra K.; Sinha, Arun K.
Tetrahedron, 2007 , vol. 63, # 39 p. 9718 - 9723
反应条件
perchloric acid T=0 - 20°C; 3 h;
参考文献
Endura S.p.A.
Patent: US6342613 B1, 2002 ;
Location in patent: Page column 6 ;
反应条件
sodium methylate Erwaermen des Reaktionsprodukts mit Salzsaeure;
参考文献
Hoering
Chemische Berichte, 1905 , vol. 38, p. 3469
Chem. Zentralbl., 1906 , vol. 77, # II p. 1223
Full Text Show Details
Wallach; Pond
Chemische Berichte, 1895 , vol. 28, p. 2719
Full Text Show Details
Hesse
Patent: DE88224 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 4, p. 1291
反应条件
phosphorus pentachloride Zerlegung des Produkts mit Wasser und Kochen des mit Wasserdampf ueberdestillierten Oels mit alkoholischer Kalilauge;
参考文献
Schimmel and Co.
Chem. Zentralbl., 1905 , vol. 76, # I p. 1470
Full Text Show Details
Schimmel and Co.
Bericht vom April 1905, 49
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone
参考文献
Kumar, Vinod; Sharma, Abhishek; Sharma, Meenakshi; Sharma, Upendra K.; Sinha, Arun K.
Tetrahedron, 2007 , vol. 63, # 39 p. 9718 - 9723
