4-乙酰氧基-2-氮杂环丁酮合成路线 (共 46 条)
反应条件
oxygen; sodium acetate; acetaldehyde; ruthenium trichloride in ethyl acetate T=40°C;
参考文献
Murahashi; Saito; Naota; Kumobayashi; Akutagawa
Tetrahedron Letters, 1991 , vol. 32, # 42 p. 5991 - 5994
反应条件
peracetic acid; sodium acetate; acetic acid in acetonitrile
参考文献
Takasago International Corporation
Patent: US5081239 A1, 1992 ;
反应条件
oxygen; sodium acetate; acetaldehyde; ruthenium trichloride in ethyl acetate T=40°C;
参考文献
Murahashi; Saito; Naota; Kumobayashi; Akutagawa
Tetrahedron Letters, 1991 , vol. 32, # 42 p. 5991 - 5994
反应条件
sodium hydrogencarbonate; sodium sulfite in dichloromethane; water T=0°C; 0.5 h;
参考文献
Lee, Sang Hyup
Bulletin of the Korean Chemical Society, 2013 , vol. 34, # 1 p. 121 - 127
反应条件
Ru-carbon; sodium acetate; acetic acid in ethyl acetate 2.5 h; Ambient temperature;
参考文献
Murahashi, Shun-Ichi; Naota, Takeshi; Kuwabara, Toshiyuki; Saito, Takao; Kumobayashi, Hidenori; Akutagawa, Susumu
Journal of the American Chemical Society, 1990 , vol. 112, # 21 p. 7820 - 7822
反应条件
Ru-carbon; sodium acetate; acetic acid in ethyl acetate 2.5 h; Ambient temperature;
参考文献
Murahashi, Shun-Ichi; Naota, Takeshi; Kuwabara, Toshiyuki; Saito, Takao; Kumobayashi, Hidenori; Akutagawa, Susumu
Journal of the American Chemical Society, 1990 , vol. 112, # 21 p. 7820 - 7822
反应条件
peracetic acid; acetic acid
参考文献
Takasago International Corporation
Patent: US5204460 A1, 1993 ;
参考文献
Crombie, Leslie; Haigh, David; Jones, Raymond C. F.; Mat-Zin, Ab. Rasid
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 17 p. 2055 - 2068
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile T=-10°C;
参考文献
Easton, Christopher J.; Love, Stephen G.; Wang, Peng
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 2 p. 277 - 282
反应条件
tetraethylammonium p-toluenesulfonate in acetonitrile Ambient temperatureconstant current electrolysis;
参考文献
Suda, Kohji; Hotoda, Katsumi; Watanabe, Jun-ichi; Shiozawa, Kei; Takanami, Toshikatsu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 11 p. 1283 - 1284