Bogoradovskii, E. T.; Zavgorodnii, V. S.; Liepin'sh, E. E.; Birgele, I. S.; Petrov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 6.2 p. 1418 - 1429,1295 - 1306
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 8 p. 1842 - 1860,1642 - 1657
→
反应条件
tetrahydrofuran in tetrahydrofuran byproducts: CO, BF3*THF, Me3SiF; N2-atmosphere; slight molar excess of Me3SiBr, stirring (50°C, 10min); sublimation off of traces Mo(CO)6; elem. anal.;
参考文献
Bochmann, Manfred; Green, Michael; Kirsch, Howard P.; Stone, F. Gordon A.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1977 , p. 714 - 718