Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Piscopo, Laura
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 3 p. 289 - 294
tetrafluoroboric acid diethyl ether complex 1.) Et2O, CH2Cl2, 0-5 deg C, 2.) r.t.; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Piscopo, Laura
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 3 p. 289 - 294
Barbero, Margherita; Degani, Iacopo; Dughera, Stefano; Fochi, Rita; Piscopo, Laura
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 3 p. 289 - 294
(i) Mg, Et2O, (ii) /BRN= 383568/; Multistep reaction;
参考文献
Dronov,V.I. et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1970 , vol. 6, p. 312 - 314
Khimiya Geterotsiklicheskikh Soedinenii, 1970 , vol. 6, p. 335 - 337
lithium diethylamide; lithium tert-butylate in tetrahydrofuran; hexane T=0°C; 6 h; other epoxides, other reagents: lithium diethylamide, lithium diisopropylamide, hexamethylphosphoroic amide, other temperature and reaction time; Mechanism;
参考文献
Saravanan, Parthasarathy; DattaGupta, Arpita; Bhuniya, Debnath; Singh, Vinod K.
Tetrahedron, 1997 , vol. 53, # 5 p. 1855 - 1860