三-O-乙酰基-D- 葡萄烯糖合成路线 （共 170 条）
反应条件
(R,R)-Pri-Pybox; diethylene glycol dimethyl ether; niobium bromide in 1,3-dimethyl-imidazolidin-2-one T=25°C; Negishi coupling reaction; 12 h;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
pyridine; terpyridine; ethylene glycol dimethyl ether; nickel dichloride in 1,3-dimethyl-imidazolidin-2-one T=25°C; Negishi coupling reaction; 12 h;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
pyridine; ethylene glycol dimethyl ether; N,N,N',N'',N''-pentamethyldiethylenetriamine; nickel dichloride in 1,3-dimethyl-imidazolidin-2-one T=25°C; Negishi coupling reaction; 12 h;
参考文献
Gong, Hegui; Gagne, Michel R.
Journal of the American Chemical Society, 2008 , vol. 130, # 36 p. 12177 - 12183
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=65 - 70°C;
参考文献
Lin, Tai-Shun; Yang, Jing-Hua; Liu, Mao-Chin; Zhu, Ju-Liang
Tetrahedron Letters, 1990 , vol. 31, # 27 p. 3829 - 3832
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene 4 h; Heating;
参考文献
Crich, David; Yao, Qingwei; Filzen, G. Fredrick
Journal of the American Chemical Society, 1995 , vol. 117, # 46 p. 11455 - 11470
反应条件
[Cp2Ti(III)Cl]2 in tetrahydrofuran Ambient temperature;
参考文献
Spencer, Roxanne P.; Cavallaro, Cullen L.; Schwartz, Jeffrey
Journal of Organic Chemistry, 1999 , vol. 64, # 11 p. 3987 - 3995
反应条件
Sulfuric acid immobilized on silica gel T=20°C; 0.333333 h; neat (no solvent);
参考文献
Zhang, Jianbo; Zhang, Bo; Zhou, Jiafen; Li, Juan; Shi, Chunjuan; Huang, Ting; Wang, Zhongfu; Tang, Jie
Journal of Carbohydrate Chemistry, 2011 , vol. 30, # 3 p. 165 - 177
反应条件
1: With hydrogen bromide; acetic acid T=20°C; 2: With sodium acetate; copper(II) sulfate; zinc in water; acetic acid Further stages.;
参考文献
Chatterjee, Nirbhik; Pandit, Palash; Halder, Samiran; Patra, Amarendra; Maiti, Dilip K.
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7775 - 7778
反应条件
carbon disulfide; Na2S*9H2O in N,N-dimethyl-formamide T=20°C; 0.0833333 h;
参考文献
Jana, Manas; Misra, Anup Kumar
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2680 - 2686
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran Ambient temperatureslow addition of SmI2;
参考文献
Doisneau, Gilles; Beau, Jean-Marie
Tetrahedron Letters, 1998 , vol. 39, # 21 p. 3477 - 3480
