反应条件
1: (1'-14C)-dodecanoic acid With N,N'-dimethyl-N,N'-propyleneurea; n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=0 - 20°C; Metallation; 1.5 h; 2: methyl iodide in tetrahydrofuran; hexane T=0 - 20°C; Methylation;
参考文献
Morigaki, Kenichi; Dallavalle, Sabrina; Walde, Peter; Colonna, Stefano; Luisi, Pier Luigi
Journal of the American Chemical Society, 1997 , vol. 119, # 2 p. 292 - 301