1-甲氧基-1,4-环己二烯合成路线 （共 44 条）
反应条件
anschliessendes Behandeln mit Aethanol;
参考文献
Wilds; Nelson
Journal of the American Chemical Society, 1953 , vol. 75, p. 5360,5364
参考文献
Krapcho; Bothner-By
Journal of the American Chemical Society, 1959 , vol. 81, p. 3658,3661, 3662, 3665
参考文献
du Pont de Nemours and Co.
Patent: US2182242 , 1938 ;
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Birch
Journal of the Chemical Society, 1944 , p. 430,432, 433, 435
Journal of the Chemical Society, 1947 , p. 1642,1647
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 102,104
反应条件
Behandeln der Reaktionsloesung mit wss. Ammoniumchlorid-Loesung;
参考文献
Birch
Journal of the Chemical Society, 1950 , p. 1551,1554
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 102,104
反应条件
in ethylene glycol under N2; mixt. of RuCl3*3H2O and MeOC6H7 (excess) in HOCH2CH2OH heated to 80°C for 3 h; stored at room temp. overnight; filtered; ppt. washed with MeOH, dried in vac.; additional portion of Rucomplex obtained by evaporating under reduced pressure the filtrate to third of vol.; elem. anal.;
参考文献
Organometallics, , vol. 24, # 10 p. 2538 - 2541
反应条件
in ethanol under N2; soln. of RuCl3*3H2O and MeOC6H7 (excess) in EtOH heated under reflux for 8 h; stored at room temp. overnight; filtered; ppt. extd. with CHCl3 (Soxlet extractor), solvent removed in vac., washed with Et2O; additional portion of Ru complex obtained by reducing the vol. of filtrate to half and refrigerating overnight; elem. anal.;
参考文献
Organometallics, , vol. 24, # 10 p. 2538 - 2541
反应条件
bromine in dichloromethane T=20°C;
参考文献
Song, Jian; Lin, Yongcheng; Szeto, Yau Shan; Chan, Wing Lai
Heterocycles, 2006 , vol. 68, # 8 p. 1685 - 1689
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 1642,1647
